1-azido-1-deoxy-2-chloro-2-deoxy-3,4,5,7-tetra-O-benzyl-D-arabino-hept-2-enoseptanoside

Base Information

• Chemical Name: 1-azido-1-deoxy-2-chloro-2-deoxy-3,4,5,7-tetra-O-benzyl-D-arabino-hept-2-enoseptanoside
• CAS No.: 1094383-30-8
• Molecular Formula: C₃₅H₃₄ClN₃O₅
• Molecular Weight: 612.125

Synonyms:1-azido-1-deoxy-2-chloro-2-deoxy-3,4,5,7-tetra-O-benzyl-D-arabino-hept-2-enoseptanoside

Chemical Property of 1-azido-1-deoxy-2-chloro-2-deoxy-3,4,5,7-tetra-O-benzyl-D-arabino-hept-2-enoseptanoside

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Technology Process of 1-azido-1-deoxy-2-chloro-2-deoxy-3,4,5,7-tetra-O-benzyl-D-arabino-hept-2-enoseptanoside

There total 1 articles about 1-azido-1-deoxy-2-chloro-2-deoxy-3,4,5,7-tetra-O-benzyl-D-arabino-hept-2-enoseptanoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

1,5-anhydro-2,3,4,6-tetra-O-benzyl-1,2-C-(dichloromethylene)-α-D-glycero-D-galacto-hexitol (1094382-79-2) → 1-azido-1-deoxy-2-chloro-2-deoxy-3,4,5,7-tetra-O-benzyl-D-arabino-hept-2-enoseptanoside (1094383-30-8)

Guidance literature:

With sodium azide; In N,N-dimethyl-formamide; at 75 ℃; for 36h;

DOI:10.1021/jo801967s

Reference yield:

1-azido-1-deoxy-2-chloro-2-deoxy-3,4,5,7-tetra-O-benzyl-D-arabino-hept-2-enoseptanoside (1094383-30-8) → C28H27N3O6

Guidance literature:

With ruthenium trichloride; sodium periodate; water; In ethyl acetate; acetonitrile; at 20 ℃; for 3h;

DOI:10.1021/jo801967s

upstream raw materials:

1,5-anhydro-2,3,4,6-tetra-O-benzyl-1,2-C-(dichloromethylene)-α-D-glycero-D-galacto-hexitol

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