tert-butyl {3-[(2-oxoethyl)thio]propyl}{2-[3-(trifluoromethyl)phenyl]ethyl}carbamate

Base Information

Chemical Name:tert-butyl {3-[(2-oxoethyl)thio]propyl}{2-[3-(trifluoromethyl)phenyl]ethyl}carbamate
CAS No.:928628-21-1
Molecular Formula:C₁₉H₂₆F₃NO₃S
Molecular Weight:405.482
Hs Code.:

Synonyms:tert-butyl {3-[(2-oxoethyl)thio]propyl}{2-[3-(trifluoromethyl)phenyl]ethyl}carbamate

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Chemical Property of tert-butyl {3-[(2-oxoethyl)thio]propyl}{2-[3-(trifluoromethyl)phenyl]ethyl}carbamate

Chemical Property:

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Technology Process of tert-butyl {3-[(2-oxoethyl)thio]propyl}{2-[3-(trifluoromethyl)phenyl]ethyl}carbamate

There total 5 articles about tert-butyl {3-[(2-oxoethyl)thio]propyl}{2-[3-(trifluoromethyl)phenyl]ethyl}carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: tert-butyl {3-[(2-hydroxyethyl)thio]propyl}{2-[3-(trifluoromethyl)phenyl]ethyl}carbamate

: 928628-21-1
tert-butyl {3-[(2-oxoethyl)thio]propyl}{2-[3-(trifluoromethyl)phenyl]ethyl}carbamate

Guidance literature:: tert-butyl {3-[(2-hydroxyethyl)thio]propyl}{2-[3-(trifluoromethyl)phenyl]ethyl}carbamate; With Dess-Martin periodane; In dichloromethane; for 1h;

With sodium hydroxide; In dichloromethane; water;

Reference yield:

: 928628-18-6
tert-butyl allyl{2-[3-(trifluoromethyl)phenyl]ethyl}carbamate

: 928628-21-1
tert-butyl {3-[(2-oxoethyl)thio]propyl}{2-[3-(trifluoromethyl)phenyl]ethyl}carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 2,2'-azobis(isobutyronitrile)

2: sulfur trioxide pyridine complex

With 2,2'-azobis(isobutyronitrile); sulfur trioxide pyridine complex;
DOI:10.1016/j.bmcl.2011.05.097

Reference yield:

: 928628-19-7
[2-(3-trifluoromethylphenyl)ethyl]carbamic acid tert-butyl ester

: 928628-21-1
tert-butyl {3-[(2-oxoethyl)thio]propyl}{2-[3-(trifluoromethyl)phenyl]ethyl}carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride

2: 2,2'-azobis(isobutyronitrile)

3: sulfur trioxide pyridine complex

With 2,2'-azobis(isobutyronitrile); sulfur trioxide pyridine complex; sodium hydride;
DOI:10.1016/j.bmcl.2011.05.097