2,3-dimethoxy-5-methyl-6-(34-bromo-35-hydroxy-3,7,11,15,19,23,27,31,35-nonamethylhexatriacont-2E,6E,10E,14E,18E,22E,26E,30E-octaenyl)-1,4-benzoquinone

Base Information

Chemical Name:2,3-dimethoxy-5-methyl-6-(34-bromo-35-hydroxy-3,7,11,15,19,23,27,31,35-nonamethylhexatriacont-2E,6E,10E,14E,18E,22E,26E,30E-octaenyl)-1,4-benzoquinone
CAS No.:96358-50-8
Molecular Formula:C₅₄H₈₃BrO₅
Molecular Weight:892.154
Hs Code.:

2,3-dimethoxy-5-methyl-6-(34-bromo-35-hydroxy-3,7,11,15,19,23,27,31,35-nonamethylhexatriacont-2E,6E,10E,14E,18E,22E,26E,30E-octaenyl)-1,4-benzoquinone

Synonyms:2,3-dimethoxy-5-methyl-6-(34-bromo-35-hydroxy-3,7,11,15,19,23,27,31,35-nonamethylhexatriacont-2E,6E,10E,14E,18E,22E,26E,30E-octaenyl)-1,4-benzoquinone

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Chemical Property of 2,3-dimethoxy-5-methyl-6-(34-bromo-35-hydroxy-3,7,11,15,19,23,27,31,35-nonamethylhexatriacont-2E,6E,10E,14E,18E,22E,26E,30E-octaenyl)-1,4-benzoquinone

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Technology Process of 2,3-dimethoxy-5-methyl-6-(34-bromo-35-hydroxy-3,7,11,15,19,23,27,31,35-nonamethylhexatriacont-2E,6E,10E,14E,18E,22E,26E,30E-octaenyl)-1,4-benzoquinone

There total 1 articles about 2,3-dimethoxy-5-methyl-6-(34-bromo-35-hydroxy-3,7,11,15,19,23,27,31,35-nonamethylhexatriacont-2E,6E,10E,14E,18E,22E,26E,30E-octaenyl)-1,4-benzoquinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 303-97-9
ubiquinone-45

: 96358-50-8
2,3-dimethoxy-5-methyl-6-(34-bromo-35-hydroxy-3,7,11,15,19,23,27,31,35-nonamethylhexatriacont-2E,6E,10E,14E,18E,22E,26E,30E-octaenyl)-1,4-benzoquinone

Guidance literature:: With N-Bromosuccinimide; water; In tetrahydrofuran; at 25 ℃; for 1h;
DOI:10.1007/BF00958351

Reference yield: 90.0%

: 96358-50-8
2,3-dimethoxy-5-methyl-6-(34-bromo-35-hydroxy-3,7,11,15,19,23,27,31,35-nonamethylhexatriacont-2E,6E,10E,14E,18E,22E,26E,30E-octaenyl)-1,4-benzoquinone

: 81914-47-8
2,3-dimethoxy-5-methyl-6-(34,35-epoxy-3,7,11,15,19,23,27,31,35-nonamethylhexatriacont-2E,6E,10E,14E,18E,22E,26E,30E-octaenyl)-1,4-benzoquinone

Guidance literature:: With potassium carbonate; In methanol; diethyl ether; at 25 ℃; for 0.666667h;
DOI:10.1007/BF00958351

Reference yield:

: 96358-50-8
2,3-dimethoxy-5-methyl-6-(34-bromo-35-hydroxy-3,7,11,15,19,23,27,31,35-nonamethylhexatriacont-2E,6E,10E,14E,18E,22E,26E,30E-octaenyl)-1,4-benzoquinone

: 303-98-0,55127-92-9
ubidecarenone

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / K₂CO₃ / methanol; diethyl ether / 0.67 h / 25 °C

2: 75 percent / 37percent HClO₄ / tetrahydrofuran; H₂O / 0.5 h / 25 °C

3: 72 percent / NaIO₄, conc. H₂SO₄ / tetrahydrofuran; H₂O / 0.5 h / 25 °C

4: tetrahydrofuran / 0.5 h / -20 °C

With sodium periodate; perchloric acid; sulfuric acid; potassium carbonate; In tetrahydrofuran; methanol; diethyl ether; water;
DOI:10.1007/BF00958351