3-(p-Nitrophenyl)-12-methyl-1,4,5,12a-tetrahydro-1,2,4-triazino<4,3-a>perimidine

Base Information

Chemical Name:3-(p-Nitrophenyl)-12-methyl-1,4,5,12a-tetrahydro-1,2,4-triazino<4,3-a>perimidine
CAS No.:111184-21-5
Molecular Formula:C₂₀H₁₇N₅O₂
Molecular Weight:359.387
Hs Code.:

Synonyms:3-(p-Nitrophenyl)-12-methyl-1,4,5,12a-tetrahydro-1,2,4-triazino<4,3-a>perimidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(p-Nitrophenyl)-12-methyl-1,4,5,12a-tetrahydro-1,2,4-triazino<4,3-a>perimidine

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Technology Process of 3-(p-Nitrophenyl)-12-methyl-1,4,5,12a-tetrahydro-1,2,4-triazino<4,3-a>perimidine

There total 3 articles about 3-(p-Nitrophenyl)-12-methyl-1,4,5,12a-tetrahydro-1,2,4-triazino<4,3-a>perimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 111184-14-6
1-Methyl-3-(p-nitrophenacyl)perimidinium Bromide

: 111184-21-5
3-(p-Nitrophenyl)-12-methyl-1,4,5,12a-tetrahydro-1,2,4-triazino<4,3-a>perimidine

Guidance literature:: With hydrazine hydrate; In methanol; at 20 ℃; for 0.5h;
DOI:10.1007/BF00473493

Reference yield:

: 99-81-0
4-Nitrophenacyl bromide

: 111184-21-5
3-(p-Nitrophenyl)-12-methyl-1,4,5,12a-tetrahydro-1,2,4-triazino<4,3-a>perimidine

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent

2: 82 percent / 99percent Hydrazine Hydrate / methanol / 0.5 h / 20 °C

With hydrazine hydrate; In methanol;
DOI:10.1007/BF00473493

Reference yield:

: 19585-93-4
1-methylperimidine

: 111184-21-5
3-(p-Nitrophenyl)-12-methyl-1,4,5,12a-tetrahydro-1,2,4-triazino<4,3-a>perimidine

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent

2: 82 percent / 99percent Hydrazine Hydrate / methanol / 0.5 h / 20 °C

With hydrazine hydrate; In methanol;
DOI:10.1007/BF00473493