Technology Process of C50H56FN7O4S
There total 8 articles about C50H56FN7O4S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine;
In
N,N-dimethyl-formamide;
at 0 - 20 ℃;
for 43h;
DOI:10.1016/j.bmcl.2012.04.032
- Guidance literature:
-
Multi-step reaction with 2 steps
1: trifluoroacetic acid
2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 43 h / 0 - 20 °C
With
1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid;
In
N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.04.032
- Guidance literature:
-
Multi-step reaction with 7 steps
1: triethylamine / tetrahydrofuran; water
2: sulfuric acid / tetrahydrofuran
3: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran
4: potassium carbonate; thiophenol / N,N-dimethyl-formamide
5: triethylamine / dichloromethane
6: trifluoroacetic acid
7: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 43 h / 0 - 20 °C
With
sulfuric acid; potassium carbonate; thiophenol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; triphenylphosphine; trifluoroacetic acid; diethylazodicarboxylate;
In
tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
3: Mitsunobu reaction;
DOI:10.1016/j.bmcl.2012.04.032
