N-[4-{[3,5-bis(trifluoromethyl)-1H-pyrazole-1-yl]methyl}phenyl]-N'-[(1-methylethyl)]-1,2-benzenedicarboxamide

Base Information

Chemical Name:N-[4-{[3,5-bis(trifluoromethyl)-1H-pyrazole-1-yl]methyl}phenyl]-N'-[(1-methylethyl)]-1,2-benzenedicarboxamide
CAS No.:1207077-48-2
Molecular Formula:C₂₃H₂₀F₆N₄O₂
Molecular Weight:498.428
Hs Code.:

Synonyms:N-[4-{[3,5-bis(trifluoromethyl)-1H-pyrazole-1-yl]methyl}phenyl]-N'-[(1-methylethyl)]-1,2-benzenedicarboxamide

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Chemical Property of N-[4-{[3,5-bis(trifluoromethyl)-1H-pyrazole-1-yl]methyl}phenyl]-N'-[(1-methylethyl)]-1,2-benzenedicarboxamide

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Technology Process of N-[4-{[3,5-bis(trifluoromethyl)-1H-pyrazole-1-yl]methyl}phenyl]-N'-[(1-methylethyl)]-1,2-benzenedicarboxamide

There total 6 articles about N-[4-{[3,5-bis(trifluoromethyl)-1H-pyrazole-1-yl]methyl}phenyl]-N'-[(1-methylethyl)]-1,2-benzenedicarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 85-44-9
phthalic anhydride

: 1207077-48-2
N-[4-{[3,5-bis(trifluoromethyl)-1H-pyrazole-1-yl]methyl}phenyl]-N'-[(1-methylethyl)]-1,2-benzenedicarboxamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetonitrile / 5 h / 20 °C / Cooling with ice

1.3: pH 2

2.1: sodium hydrogencarbonate; methyl chloroformate / water; ethyl acetate / 0.33 h / 50 °C

3.1: toluene-4-sulfonic acid / acetonitrile / 3 h / 20 °C

With sodium hydrogencarbonate; methyl chloroformate; toluene-4-sulfonic acid; In water; ethyl acetate; acetonitrile;

Reference yield:

: 4-{[3,5-bis(trifluoromethyl)-1H-pyrazol-1-yl]methyl}aniline

: 103606-36-6
3-(isopropylimino)-2-benzofuran-1(3H)-one

: 1207077-48-2
N-[4-{[3,5-bis(trifluoromethyl)-1H-pyrazole-1-yl]methyl}phenyl]-N'-[(1-methylethyl)]-1,2-benzenedicarboxamide

Guidance literature:: toluene-4-sulfonic acid; In acetonitrile; at 20 ℃; for 3h;

Reference yield:

: 20320-33-6
2-(isopropylcarbamoyl)benzoic acid

: 1207077-48-2
N-[4-{[3,5-bis(trifluoromethyl)-1H-pyrazole-1-yl]methyl}phenyl]-N'-[(1-methylethyl)]-1,2-benzenedicarboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate; methyl chloroformate / water; ethyl acetate / 0.33 h / 50 °C

2: toluene-4-sulfonic acid / acetonitrile / 3 h / 20 °C

With sodium hydrogencarbonate; methyl chloroformate; toluene-4-sulfonic acid; In water; ethyl acetate; acetonitrile;