2-(6-chloro-3-imino-[1,2,4]triazolo[4,3-b]pyridazin-2-yl)-1-(3,5-di-tert-butyl-4-hydroxyphenyl)ethanone trifluoroacetate

Base Information

Chemical Name:2-(6-chloro-3-imino-[1,2,4]triazolo[4,3-b]pyridazin-2-yl)-1-(3,5-di-tert-butyl-4-hydroxyphenyl)ethanone trifluoroacetate
CAS No.:1178578-27-2
Molecular Formula:C₂HF₃O₂*C₂₁H₂₆ClN₅O₂
Molecular Weight:529.947
Hs Code.:

Synonyms:2-(6-chloro-3-imino-[1,2,4]triazolo[4,3-b]pyridazin-2-yl)-1-(3,5-di-tert-butyl-4-hydroxyphenyl)ethanone trifluoroacetate

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Chemical Property of 2-(6-chloro-3-imino-[1,2,4]triazolo[4,3-b]pyridazin-2-yl)-1-(3,5-di-tert-butyl-4-hydroxyphenyl)ethanone trifluoroacetate

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Technology Process of 2-(6-chloro-3-imino-[1,2,4]triazolo[4,3-b]pyridazin-2-yl)-1-(3,5-di-tert-butyl-4-hydroxyphenyl)ethanone trifluoroacetate

There total 2 articles about 2-(6-chloro-3-imino-[1,2,4]triazolo[4,3-b]pyridazin-2-yl)-1-(3,5-di-tert-butyl-4-hydroxyphenyl)ethanone trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 14386-64-2
2-bromo-1-(3,5-di-tert-butyl-4-hydroxyphenyl)ethanone

: 53890-39-4
6-chloro-[1,2,4]triazolo[4,3-b]pyridazin-3-amine

: 76-05-1
trifluoroacetic acid

: 1178578-27-2
2-(6-chloro-3-imino-[1,2,4]triazolo[4,3-b]pyridazin-2-yl)-1-(3,5-di-tert-butyl-4-hydroxyphenyl)ethanone trifluoroacetate

Guidance literature:: 2-bromo-1-(3,5-di-tert-butyl-4-hydroxyphenyl)ethanone; 6-chloro-[1,2,4]triazolo[4,3-b]pyridazin-3-ylamine; In N,N-dimethyl-formamide; at 20 - 60 ℃; Inert atmosphere;

trifluoroacetic acid; In water; acetonitrile;

Reference yield:

: 1178583-12-4
6-chloro-[1,2,4]triazolo[4,3-b]pyridazin-3-ylamine hydrobromide

: 1178578-27-2
2-(6-chloro-3-imino-[1,2,4]triazolo[4,3-b]pyridazin-2-yl)-1-(3,5-di-tert-butyl-4-hydroxyphenyl)ethanone trifluoroacetate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / water / Inert atmosphere

2: N,N-dimethyl-formamide / 20 - 60 °C / Inert atmosphere

With potassium carbonate; In water; N,N-dimethyl-formamide;