1-acetyl-3-(2,3-di-O-acetyl-5-O-p-nitrobenzoyl-β-D-ribofuranosyl)-6-nitroindole

Base Information

Chemical Name:1-acetyl-3-(2,3-di-O-acetyl-5-O-p-nitrobenzoyl-β-D-ribofuranosyl)-6-nitroindole
CAS No.:76540-91-5
Molecular Formula:C₂₆H₂₃N₃O₁₂
Molecular Weight:569.482
Hs Code.:

Synonyms:1-acetyl-3-(2,3-di-O-acetyl-5-O-p-nitrobenzoyl-β-D-ribofuranosyl)-6-nitroindole

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Chemical Property of 1-acetyl-3-(2,3-di-O-acetyl-5-O-p-nitrobenzoyl-β-D-ribofuranosyl)-6-nitroindole

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Technology Process of 1-acetyl-3-(2,3-di-O-acetyl-5-O-p-nitrobenzoyl-β-D-ribofuranosyl)-6-nitroindole

There total 5 articles about 1-acetyl-3-(2,3-di-O-acetyl-5-O-p-nitrobenzoyl-β-D-ribofuranosyl)-6-nitroindole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 108-24-7
acetic anhydride

: 76540-90-4
3-(5-O-p-nitrobenzoyl-β-D-ribofuranosyl)-6-nitroindole

: 76540-91-5
1-acetyl-3-(2,3-di-O-acetyl-5-O-p-nitrobenzoyl-β-D-ribofuranosyl)-6-nitroindole

Guidance literature:: With pyridine; at 20 ℃; for 12h;
DOI:10.1007/BF00503480 DOI:10.1016/S0008-6215(00)80749-1

Reference yield:

: 4769-96-4
6-nitroindole

: 76540-91-5
1-acetyl-3-(2,3-di-O-acetyl-5-O-p-nitrobenzoyl-β-D-ribofuranosyl)-6-nitroindole

Guidance literature:: Multi-step reaction with 3 steps

1: 29 percent / Ag₂O / benzene / 20 h

2: 89 percent / 10 M hydrochloric acid / methanol / 1 h / 20 °C

3: 63 percent / pyridine / 12 h / 20 °C

With pyridine; hydrogenchloride; silver(l) oxide; In methanol; benzene;
DOI:10.1016/S0008-6215(00)80749-1

Reference yield:

: 74464-86-1
bromo-1 O-isopropylidene-2,3 O-paranitrobenzoyl-5-D-ribofurannose

: 76540-91-5
1-acetyl-3-(2,3-di-O-acetyl-5-O-p-nitrobenzoyl-β-D-ribofuranosyl)-6-nitroindole

Guidance literature:: Multi-step reaction with 3 steps

1: 29 percent / Ag₂O / benzene / 20 h

2: 89 percent / 10 M hydrochloric acid / methanol / 1 h / 20 °C

3: 63 percent / pyridine / 12 h / 20 °C

With pyridine; hydrogenchloride; silver(l) oxide; In methanol; benzene;
DOI:10.1016/S0008-6215(00)80749-1