(S)-ethyl 3-(3-methylphenyl)butanoate

Base Information

Chemical Name:(S)-ethyl 3-(3-methylphenyl)butanoate
CAS No.:130378-45-9
Molecular Formula:C₁₃H₁₈O₂
Molecular Weight:206.285
Hs Code.:

Synonyms:(S)-ethyl 3-(3-methylphenyl)butanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-ethyl 3-(3-methylphenyl)butanoate

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Technology Process of (S)-ethyl 3-(3-methylphenyl)butanoate

There total 10 articles about (S)-ethyl 3-(3-methylphenyl)butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 433732-56-0
(E)-ethyl 3-(3-methylphenyl)-but-2-enoate

: 130378-45-9
(S)-ethyl 3-(3-methylphenyl)butanoate

Guidance literature:: With nickel(II) bromide dimethoxyethane; indium; water; tetra-(n-butyl)ammonium iodide; acetic acid; [2R-[1(2'R*,5'R*),2a,5b]]-1,1'-(1,2-phenylene)bis[2,5-dimethylphospholane]; In tetrahydrofuran; at 80 ℃; for 24h; enantioselective reaction; Glovebox; Inert atmosphere; Schlenk technique;
DOI:10.1021/acs.orglett.0c00112

Reference yield: 92.0%

: C₁₃H₁₆O₂

: 130378-45-9
(S)-ethyl 3-(3-methylphenyl)butanoate

Guidance literature:: With aluminum (III) chloride; nickel(II) bromide dimethoxyethane; N,N-dimethyl-formamide; [2R-[1(2'R*,5'R*),2a,5b]]-1,1'-(1,2-phenylene)bis[2,5-dimethylphospholane]; In water; at 110 ℃; for 24h; Inert atmosphere; Glovebox; Schlenk technique;
DOI:10.1021/acs.orglett.6b02662

Reference yield:

: 1286204-30-5
(+/-)-ethyl 3-(3-methylphenyl)butanoate

: 1286694-65-2
(R)-3-(3-methylphenyl)butanoic acid

: 836655-29-9
(S)-3-(3-methylphenyl)butanoic acid

: 130378-45-9
(S)-ethyl 3-(3-methylphenyl)butanoate

Guidance literature:: With immobilized Candida antarctica Lipase B; water; at 30 ℃; for 65h; pH=7; optical yield given as %ee; enantioselective reaction; aq. phosphate buffer; Enzymatic reaction;
DOI:10.1016/j.tetasy.2010.12.019