C₂₈⁽¹³⁾CH₃₉NO₄S

Base Information Edit

Chemical Name:C₂₈⁽¹³⁾CH₃₉NO₄S
CAS No.:263710-60-7
Molecular Formula:C₂₉H₃₉NO₄S
Molecular Weight:498.688
Hs Code.:
Mol file:263710-60-7.mol

C<sub>28</sub><sup>(13)</sup>CH<sub>39</sub>NO<sub>4</sub>S

Synonyms:C₂₈⁽¹³⁾CH₃₉NO₄S

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Chemical Property of C₂₈⁽¹³⁾CH₃₉NO₄S Edit

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of C₂₈⁽¹³⁾CH₃₉NO₄S

There total 2 articles about C₂₈⁽¹³⁾CH₃₉NO₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 4227-95-6
[13C]methyl iodide

: 102834-10-6
(E)-But-2-enoic acid (1R,2S,3R,4S)-3-[benzenesulfonyl-(3,5-dimethyl-phenyl)-amino]-1,7,7-trimethyl-bicyclo[2.2.1]hept-2-yl ester

: 263710-60-7
C₂₈⁽¹³⁾CH₃₉NO₄S

Guidance literature:: [13C]methyl iodide; With lithium; In diethyl ether; at 0 - 20 ℃; for 5h;

With copper(l) iodide; In diethyl ether; toluene; at -10 ℃; for 0.333333h;

(E)-But-2-enoic acid (1R,2S,3R,4S)-3-[benzenesulfonyl-(3,5-dimethyl-phenyl)-amino]-1,7,7-trimethyl-bicyclo[2.2.1]hept-2-yl ester; With boron trifluoride diethyl etherate; In diethyl ether; toluene; at -78 - -20 ℃; for 7h; Further stages.;

Reference yield:

: 87420-26-6
(1R,2S,3R)-3-[N-Phenylsulfonyl-N-(3,5-dimethylphenyl)amino]bornan-2-ol

: 263710-60-7
C₂₈⁽¹³⁾CH₃₉NO₄S

Guidance literature:: Multi-step reaction with 2 steps

1.1: 81 percent / molecular sieves 4 Angstroem / CCl₄ / Heating

2.1: Li / diethyl ether / 5 h / 0 - 20 °C

2.2: CuI / diethyl ether; toluene / 0.33 h / -10 °C

2.3: 79 percent / BF₃*OEt₂ / diethyl ether; toluene / 7 h / -78 - -20 °C

With 4 A molecular sieve; lithium; In tetrachloromethane; diethyl ether; 1.1: Esterification / 2.1: Metallation / 2.2: Metallation / 2.3: Methylation;