1,4-bis(2,6-diethylphenyl)-1,4-diazabuta-1,3-diene

Base Information

Chemical Name:1,4-bis(2,6-diethylphenyl)-1,4-diazabuta-1,3-diene
CAS No.:290333-55-0
Molecular Formula:C₂₂H₂₈N₂
Molecular Weight:320.478
Hs Code.:

Synonyms:1,4-bis(2,6-diethylphenyl)-1,4-diazabuta-1,3-diene

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Chemical Property of 1,4-bis(2,6-diethylphenyl)-1,4-diazabuta-1,3-diene

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Technology Process of 1,4-bis(2,6-diethylphenyl)-1,4-diazabuta-1,3-diene

There total 1 articles about 1,4-bis(2,6-diethylphenyl)-1,4-diazabuta-1,3-diene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 579-66-8
2,6-diethylaniline

: 131543-46-9,107-22-2
Glyoxal

: 290333-55-0
1,4-bis(2,6-diethylphenyl)-1,4-diazabuta-1,3-diene

Guidance literature:: With formic acid; In ethanol; water; at 20 ℃; for 18h;
DOI:10.1016/j.tetlet.2013.06.132

Reference yield: 97.0%

: 290333-55-0
1,4-bis(2,6-diethylphenyl)-1,4-diazabuta-1,3-diene

: 1030868-43-9
[BeI₂(OEt₂)₂]

: [((2,6-diethylphenyl-NCH)₂)BeI₂]

Guidance literature:: In toluene; at 20 ℃; for 0.166667h; Schlenk technique; Inert atmosphere;
DOI:10.1002/asia.201801800

Reference yield: 91.0%

: pentamethylcyclopentadienylgallium(I)

: 290333-55-0
1,4-bis(2,6-diethylphenyl)-1,4-diazabuta-1,3-diene

: [(η1-Cp*)GaN(Dep)CH=CHN(Dep)]

Guidance literature:: In tetrahydrofuran; under Ar atm. Cp*Ga was added to stirred soln. Dep-DAB in THF at room temp., react. mixt. was stirred for 1 h; volatile components were removed in vacuo; elem. anal.;
DOI:10.1021/om001045b