Technology Process of C54H48B2F10N6O2S2
There total 6 articles about C54H48B2F10N6O2S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
boron trifluoride diethyl etherate; N-ethyl-N,N-diisopropylamine;
In
dichloromethane;
for 0.166667h;
Reflux;
DOI:10.1002/ejoc.201100108
- Guidance literature:
-
Multi-step reaction with 2 steps
1: trichlorophosphate / Inert atmosphere; Reflux
2: boron trifluoride diethyl etherate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.17 h / Reflux
With
boron trifluoride diethyl etherate; N-ethyl-N,N-diisopropylamine; trichlorophosphate;
In
dichloromethane;
DOI:10.1002/ejoc.201100108
- Guidance literature:
-
Multi-step reaction with 5 steps
1: isopentyl nitrite / tetrahydrofuran / 0.5 h / Reflux
2: hydrazine hydrate / ethanol / 1.5 h / Reflux
3: acetic acid / ethanol / 120 h / 20 °C
4: trichlorophosphate / Inert atmosphere; Reflux
5: boron trifluoride diethyl etherate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.17 h / Reflux
With
boron trifluoride diethyl etherate; hydrazine hydrate; acetic acid; N-ethyl-N,N-diisopropylamine; trichlorophosphate; isopentyl nitrite;
In
tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1002/ejoc.201100108