N-[4-(1,1,1,2,3,3,3-heptafluoropropan-2-yl)-2,6-dimethylphenyl]quinoline-6-carboxamide-1-oxide

Base Information

Chemical Name:N-[4-(1,1,1,2,3,3,3-heptafluoropropan-2-yl)-2,6-dimethylphenyl]quinoline-6-carboxamide-1-oxide
CAS No.:1262663-57-9
Molecular Formula:C₂₁H₁₅F₇N₂O₂
Molecular Weight:460.351
Hs Code.:

Synonyms:N-[4-(1,1,1,2,3,3,3-heptafluoropropan-2-yl)-2,6-dimethylphenyl]quinoline-6-carboxamide-1-oxide

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Chemical Property of N-[4-(1,1,1,2,3,3,3-heptafluoropropan-2-yl)-2,6-dimethylphenyl]quinoline-6-carboxamide-1-oxide

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Technology Process of N-[4-(1,1,1,2,3,3,3-heptafluoropropan-2-yl)-2,6-dimethylphenyl]quinoline-6-carboxamide-1-oxide

There total 3 articles about N-[4-(1,1,1,2,3,3,3-heptafluoropropan-2-yl)-2,6-dimethylphenyl]quinoline-6-carboxamide-1-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1262663-56-8
N-[4-(1,1,1,2,3,3,3-heptafluoropropan-2-yl)-2,6-dimethylphenyl]quinoline-6-carboxamide

: 1262663-57-9
N-[4-(1,1,1,2,3,3,3-heptafluoropropan-2-yl)-2,6-dimethylphenyl]quinoline-6-carboxamide-1-oxide

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 18 - 30 ℃; for 3h;

Reference yield:

: 72369-87-0
quinoline-6-carbonyl chloride

: 1262663-57-9
N-[4-(1,1,1,2,3,3,3-heptafluoropropan-2-yl)-2,6-dimethylphenyl]quinoline-6-carboxamide-1-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / dichloromethane / 5 h / 18 - 30 °C

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 3 h / 18 - 30 °C

With pyridine; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;

Reference yield:

: 10349-57-2
Quinoline-6-carboxylic acid

: 1262663-57-9
N-[4-(1,1,1,2,3,3,3-heptafluoropropan-2-yl)-2,6-dimethylphenyl]quinoline-6-carboxamide-1-oxide

Guidance literature:: Multi-step reaction with 3 steps

1: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 2.33 h / 18 - 30 °C / Reflux

2: pyridine / dichloromethane / 5 h / 18 - 30 °C

3: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 3 h / 18 - 30 °C

With pyridine; oxalyl dichloride; N,N-dimethyl-formamide; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;