1-(5-((1R,2R)-2-(benzyloxycarbonylamino)cyclohexylamino)-5-oxopentyl)-3-methyl-1H-imidazol-3-ium hexafluorophosphate

Base Information

Chemical Name:1-(5-((1R,2R)-2-(benzyloxycarbonylamino)cyclohexylamino)-5-oxopentyl)-3-methyl-1H-imidazol-3-ium hexafluorophosphate
CAS No.:1438415-84-9
Molecular Formula:C₂₃H₃₃N₄O₃*F₆P
Molecular Weight:558.504
Hs Code.:

Synonyms:1-(5-((1R,2R)-2-(benzyloxycarbonylamino)cyclohexylamino)-5-oxopentyl)-3-methyl-1H-imidazol-3-ium hexafluorophosphate

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Chemical Property of 1-(5-((1R,2R)-2-(benzyloxycarbonylamino)cyclohexylamino)-5-oxopentyl)-3-methyl-1H-imidazol-3-ium hexafluorophosphate

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Technology Process of 1-(5-((1R,2R)-2-(benzyloxycarbonylamino)cyclohexylamino)-5-oxopentyl)-3-methyl-1H-imidazol-3-ium hexafluorophosphate

There total 4 articles about 1-(5-((1R,2R)-2-(benzyloxycarbonylamino)cyclohexylamino)-5-oxopentyl)-3-methyl-1H-imidazol-3-ium hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1438415-82-7
1-(5-((1R,2R)-2-(benzyloxycarbonylamino)cyclohexylamino)-5-oxopentyl)-3-methyl-1H-imidazol-3-ium bromide

: 1438415-84-9
1-(5-((1R,2R)-2-(benzyloxycarbonylamino)cyclohexylamino)-5-oxopentyl)-3-methyl-1H-imidazol-3-ium hexafluorophosphate

Guidance literature:: With potassium hexafluorophosphate; In water;
DOI:10.1002/adsc.201200338

Reference yield:

: 1438415-81-6
benzyl (1R,2R)-2-(5-bromopentanamido)cyclohexylcarbamate

: 1438415-84-9
1-(5-((1R,2R)-2-(benzyloxycarbonylamino)cyclohexylamino)-5-oxopentyl)-3-methyl-1H-imidazol-3-ium hexafluorophosphate

Guidance literature:: Multi-step reaction with 2 steps

1: 0.17 h / 80 °C

2: potassium hexafluorophosphate / water

With potassium hexafluorophosphate; In water;
DOI:10.1002/adsc.201200338

Reference yield:

: 28170-07-2
benzyl phenyl carbonate

: 1438415-84-9
1-(5-((1R,2R)-2-(benzyloxycarbonylamino)cyclohexylamino)-5-oxopentyl)-3-methyl-1H-imidazol-3-ium hexafluorophosphate

Guidance literature:: Multi-step reaction with 4 steps

1: ethanol / 24 h / 20 °C

2: triethylamine / tetrahydrofuran / 2 h / 5 - 20 °C

3: 0.17 h / 80 °C

4: potassium hexafluorophosphate / water

With potassium hexafluorophosphate; triethylamine; In tetrahydrofuran; ethanol; water;
DOI:10.1002/adsc.201200338