(4,5-dimethoxy-2-nitrophenyl)[4-(1,4-dioxa-7,13-dithia-10-azacyclopentadecan-10-yl)phenyl]methanol

Base Information

• Chemical Name: (4,5-dimethoxy-2-nitrophenyl)[4-(1,4-dioxa-7,13-dithia-10-azacyclopentadecan-10-yl)phenyl]methanol
• CAS No.: 1260103-51-2
• Molecular Formula: C₂₅H₃₄N₂O₇S₂
• Molecular Weight: 538.686

Synonyms:(4,5-dimethoxy-2-nitrophenyl)[4-(1,4-dioxa-7,13-dithia-10-azacyclopentadecan-10-yl)phenyl]methanol

Chemical Property of (4,5-dimethoxy-2-nitrophenyl)[4-(1,4-dioxa-7,13-dithia-10-azacyclopentadecan-10-yl)phenyl]methanol

Chemical Property:

Purity/Quality:

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Technology Process of (4,5-dimethoxy-2-nitrophenyl)[4-(1,4-dioxa-7,13-dithia-10-azacyclopentadecan-10-yl)phenyl]methanol

There total 3 articles about (4,5-dimethoxy-2-nitrophenyl)[4-(1,4-dioxa-7,13-dithia-10-azacyclopentadecan-10-yl)phenyl]methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

C28H42N2O7S2Si → (4,5-dimethoxy-2-nitrophenyl)[4-(1,4-dioxa-7,13-dithia-10-azacyclopentadecan-10-yl)phenyl]methanol (1260103-51-2)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; dichloromethane; for 0.0833333h;

DOI:10.1002/ejic.201000673

Reference yield:

6-nitroveratraldehyde (20357-25-9) → (4,5-dimethoxy-2-nitrophenyl)[4-(1,4-dioxa-7,13-dithia-10-azacyclopentadecan-10-yl)phenyl]methanol (1260103-51-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 2,6-di-tert-butyl-4-methylpyridine / dichloromethane / 16 h / 23 °C

2: tetrabutyl ammonium fluoride / tetrahydrofuran; dichloromethane / 0.08 h

With 2,6-di-tert-butyl-4-methylpyridine; tetrabutyl ammonium fluoride; In tetrahydrofuran; dichloromethane;

DOI:10.1002/ejic.201000673

Reference yield:

10-phenyl-1,4-dioxa-7,13-dithia-10-aza-cyclopentadecane (240797-81-3) → (4,5-dimethoxy-2-nitrophenyl)[4-(1,4-dioxa-7,13-dithia-10-azacyclopentadecan-10-yl)phenyl]methanol (1260103-51-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 2,6-di-tert-butyl-4-methylpyridine / dichloromethane / 16 h / 23 °C

2: tetrabutyl ammonium fluoride / tetrahydrofuran; dichloromethane / 0.08 h

With 2,6-di-tert-butyl-4-methylpyridine; tetrabutyl ammonium fluoride; In tetrahydrofuran; dichloromethane;

DOI:10.1002/ejic.201000673

upstream raw materials:

6-nitroveratraldehyde

10-phenyl-1,4-dioxa-7,13-dithia-10-aza-cyclopentadecane

Downstream raw materials:

Hg((C₂H₄O)2(C₂H₄S)2C₂H₄NC₆H₄CHOHC₆H₂(NO₂)(OCH₃)2)ClO₄⁽¹⁺⁾*ClO₄^(1-)=Hg(C₂H₄O)2(C₂H₄S)2C₂H₄NC₆H₄CHOHC₆H₂NO₂(OCH₃)2(ClO₄)2

(4,5-dimethoxy-2-nitrosophenyl)[4-(1,4-dioxa-7,13-dithia-10-azacyclopentadecan-10-yl)phenyl]methanone

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