6-Acetamido-3-O-benzyl-5,7-O-benzyliden-6-desoxy-1,2-O-isopropyliden-D-glycero-α-D-gluco-heptofuranose

Base Information

Chemical Name:6-Acetamido-3-O-benzyl-5,7-O-benzyliden-6-desoxy-1,2-O-isopropyliden-D-glycero-α-D-gluco-heptofuranose
CAS No.:95580-86-2
Molecular Formula:C₂₆H₃₁NO₇
Molecular Weight:469.535
Hs Code.:

Synonyms:6-Acetamido-3-O-benzyl-5,7-O-benzyliden-6-desoxy-1,2-O-isopropyliden-D-glycero-α-D-gluco-heptofuranose

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Chemical Property of 6-Acetamido-3-O-benzyl-5,7-O-benzyliden-6-desoxy-1,2-O-isopropyliden-D-glycero-α-D-gluco-heptofuranose

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Technology Process of 6-Acetamido-3-O-benzyl-5,7-O-benzyliden-6-desoxy-1,2-O-isopropyliden-D-glycero-α-D-gluco-heptofuranose

There total 6 articles about 6-Acetamido-3-O-benzyl-5,7-O-benzyliden-6-desoxy-1,2-O-isopropyliden-D-glycero-α-D-gluco-heptofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1125-88-8
benzaldehyde dimethyl acetal

: 95580-81-7
6-Acetamido-3-O-benzyl-6-desoxy-1,2-O-isopropyliden-D-glycero-α-D-gluco-heptofuranose

: 95580-86-2
6-Acetamido-3-O-benzyl-5,7-O-benzyliden-6-desoxy-1,2-O-isopropyliden-D-glycero-α-D-gluco-heptofuranose

Guidance literature:: With toluene-4-sulfonic acid; In acetonitrile; for 5h; Ambient temperature;

Reference yield: 14.4%

: 1125-88-8
benzaldehyde dimethyl acetal

: 95580-81-7
6-Acetamido-3-O-benzyl-6-desoxy-1,2-O-isopropyliden-D-glycero-α-D-gluco-heptofuranose

: 95580-86-2
6-Acetamido-3-O-benzyl-5,7-O-benzyliden-6-desoxy-1,2-O-isopropyliden-D-glycero-α-D-gluco-heptofuranose

: 95580-87-3
6-Acetamido-3-O-benzyl-5,7-O-benzyliden-6-desoxy-1,2-O-isopropyliden-D-glycero-α-D-gluco-heptofuranose

Guidance literature:: With toluene-4-sulfonic acid; In acetonitrile; for 4h; Ambient temperature;
DOI:10.1002/jlac.198519850113

Reference yield:

: 107222-85-5,107222-86-6
2-Benzyloxycarbonylamino-3-((3aR,5R,6S,6aR)-6-benzyloxy-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-5-yl)-3-hydroxy-propionic acid

: 95580-86-2
6-Acetamido-3-O-benzyl-5,7-O-benzyliden-6-desoxy-1,2-O-isopropyliden-D-glycero-α-D-gluco-heptofuranose

Guidance literature:: Multi-step reaction with 4 steps

1: diethyl ether; methanol

2: 86 percent / H₂ / Raney-nickel / methanol / 2 h

3: 62 percent / LiAlH₄ / tetrahydrofuran / 4 h / Ambient temperature

4: 87 percent / toluen-4-sulfonic acid / acetonitrile / 5 h / Ambient temperature

With lithium aluminium tetrahydride; hydrogen; toluene-4-sulfonic acid; nickel; In tetrahydrofuran; methanol; diethyl ether; acetonitrile;