C₃₆H₄₃N₃O₉SSe

Base Information

Chemical Name:C₃₆H₄₃N₃O₉SSe
CAS No.:566905-23-5
Molecular Formula:C₃₆H₄₃N₃O₉SSe
Molecular Weight:772.778
Hs Code.:

C<sub>36</sub>H<sub>43</sub>N<sub>3</sub>O<sub>9</sub>SSe

Synonyms:C₃₆H₄₃N₃O₉SSe

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Chemical Property of C₃₆H₄₃N₃O₉SSe

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Technology Process of C₃₆H₄₃N₃O₉SSe

There total 20 articles about C₃₆H₄₃N₃O₉SSe which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 390748-07-9
ethyl 3-[4-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)-2-furyl]propanoate

: 566905-23-5
C₃₆H₄₃N₃O₉SSe

Guidance literature:: Multi-step reaction with 12 steps

1: 95 percent / K₃PO₄; PdCl₂(dppf) / dimethylformamide / 3 h / 80 °C

2: 92 percent / Pd/C / methanol / 1.5 h / 20 °C

3: 72 percent / PPTS; EtOH / methanol / 3 h / 50 °C

4: 96 percent / CSA / CH₂Cl₂ / 1.5 h / 20 °C

5: 94 percent / LiBH₄ / methanol; tetrahydrofuran / 19 h / 3 - 20 °C

6: lithium / tetrahydrofuran; liquid ammonia / 0.5 h / -78 °C

7: 5.71 g / aq. NaHCO₃ / ethyl acetate / 1 h / 20 °C

8: 68 percent / DMAP; Et₃N / tetrahydrofuran / 11 h / 20 °C

9: DIBAL-H / toluene; CH₂Cl₂ / 2 h / -78 - 20 °C

10: 7.57 g / pyridine / 12 h / 20 °C

11: 37 percent / p-TsOH monohydrate / CH₂Cl₂ / 1.2 h / 20 °C

12: tri-n-butylphosphine / tetrahydrofuran / 16 h / 20 °C

With dmap; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate; lithium borohydride; ethanol; tributylphosphine; camphor-10-sulfonic acid; pyridinium p-toluenesulfonate; lithium; diisobutylaluminium hydride; sodium hydrogencarbonate; toluene-4-sulfonic acid; triethylamine; palladium on activated charcoal; In tetrahydrofuran; pyridine; methanol; dichloromethane; ammonia; ethyl acetate; N,N-dimethyl-formamide; toluene; 1: Suzuki-Miyaura coupling;
DOI:10.1021/ja034464j

Reference yield:

: 390748-06-8
ethyl 3-(4-bromo-2-furyl)propanoate

: 566905-23-5
C₃₆H₄₃N₃O₉SSe

Guidance literature:: Multi-step reaction with 13 steps

1: 82 percent / potasium acetate; PdCl₂(dppf) / dimethylsulfoxide / 5 h / 82 °C

2: 95 percent / K₃PO₄; PdCl₂(dppf) / dimethylformamide / 3 h / 80 °C

3: 92 percent / Pd/C / methanol / 1.5 h / 20 °C

4: 72 percent / PPTS; EtOH / methanol / 3 h / 50 °C

5: 96 percent / CSA / CH₂Cl₂ / 1.5 h / 20 °C

6: 94 percent / LiBH₄ / methanol; tetrahydrofuran / 19 h / 3 - 20 °C

7: lithium / tetrahydrofuran; liquid ammonia / 0.5 h / -78 °C

8: 5.71 g / aq. NaHCO₃ / ethyl acetate / 1 h / 20 °C

9: 68 percent / DMAP; Et₃N / tetrahydrofuran / 11 h / 20 °C

10: DIBAL-H / toluene; CH₂Cl₂ / 2 h / -78 - 20 °C

11: 7.57 g / pyridine / 12 h / 20 °C

12: 37 percent / p-TsOH monohydrate / CH₂Cl₂ / 1.2 h / 20 °C

13: tri-n-butylphosphine / tetrahydrofuran / 16 h / 20 °C

With dmap; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate; lithium borohydride; ethanol; tributylphosphine; camphor-10-sulfonic acid; potassium acetate; pyridinium p-toluenesulfonate; lithium; diisobutylaluminium hydride; sodium hydrogencarbonate; toluene-4-sulfonic acid; triethylamine; palladium on activated charcoal; In tetrahydrofuran; pyridine; methanol; dichloromethane; ammonia; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide; toluene; 2: Suzuki-Miyaura coupling;
DOI:10.1021/ja034464j

Reference yield:

: 566905-10-0
(3S,5R)-2-benzyl-3-(2-hydroxyethyl)-7-(phenylsulfonyl)-2,7-diazaspiro[4.5]decane-1,10-dione

: 566905-23-5
C₃₆H₄₃N₃O₉SSe

Guidance literature:: Multi-step reaction with 14 steps

1.1: 90 percent / CSA / CH₂Cl₂ / 1.5 h / 20 °C

2.1: lithium bis(trimethylsilyl)amide / tetrahydrofuran / 0.75 h / -78 °C

2.2: 92 percent / tetrahydrofuran / 13 h / 20 °C

3.1: 95 percent / K₃PO₄; PdCl₂(dppf) / dimethylformamide / 3 h / 80 °C

4.1: 92 percent / Pd/C / methanol / 1.5 h / 20 °C

5.1: 72 percent / PPTS; EtOH / methanol / 3 h / 50 °C

6.1: 96 percent / CSA / CH₂Cl₂ / 1.5 h / 20 °C

7.1: 94 percent / LiBH₄ / methanol; tetrahydrofuran / 19 h / 3 - 20 °C

8.1: lithium / tetrahydrofuran; liquid ammonia / 0.5 h / -78 °C

9.1: 5.71 g / aq. NaHCO₃ / ethyl acetate / 1 h / 20 °C

10.1: 68 percent / DMAP; Et₃N / tetrahydrofuran / 11 h / 20 °C

11.1: DIBAL-H / toluene; CH₂Cl₂ / 2 h / -78 - 20 °C

12.1: 7.57 g / pyridine / 12 h / 20 °C

13.1: 37 percent / p-TsOH monohydrate / CH₂Cl₂ / 1.2 h / 20 °C

14.1: tri-n-butylphosphine / tetrahydrofuran / 16 h / 20 °C

With dmap; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate; lithium borohydride; ethanol; tributylphosphine; camphor-10-sulfonic acid; pyridinium p-toluenesulfonate; lithium; diisobutylaluminium hydride; sodium hydrogencarbonate; toluene-4-sulfonic acid; triethylamine; lithium hexamethyldisilazane; palladium on activated charcoal; In tetrahydrofuran; pyridine; methanol; dichloromethane; ammonia; ethyl acetate; N,N-dimethyl-formamide; toluene; 3.1: Suzuki-Miyaura coupling;
DOI:10.1021/ja034464j