D-glycero-D-gulo-Dec-2-enitol, 1,6:5,9-dianhydro-2,3,4-trideoxy- (9CI)

Base Information

Chemical Name:D-glycero-D-gulo-Dec-2-enitol, 1,6:5,9-dianhydro-2,3,4-trideoxy- (9CI)
CAS No.:440320-43-4
Molecular Formula:C10H16 O5
Molecular Weight:216.23104
Hs Code.:
Mol file:440320-43-4.mol

Synonyms:D-glycero-D-gulo-Dec-2-enitol, 1,6:5,9-dianhydro-2,3,4-trideoxy- (9CI)

Suppliers and Price of D-glycero-D-gulo-Dec-2-enitol, 1,6:5,9-dianhydro-2,3,4-trideoxy- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of D-glycero-D-gulo-Dec-2-enitol, 1,6:5,9-dianhydro-2,3,4-trideoxy- (9CI)

Chemical Property:

PSA：79.15000
LogP:-1.18700

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of D-glycero-D-gulo-Dec-2-enitol, 1,6:5,9-dianhydro-2,3,4-trideoxy- (9CI)

There total 6 articles about D-glycero-D-gulo-Dec-2-enitol, 1,6:5,9-dianhydro-2,3,4-trideoxy- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 252046-22-3
(2R,3R,4S,4aS,9aS)-3,4-bis(benzyloxy)-2-(benzyloxymethyl)-2,3,4,4a,9,9a-hexahydro-6H-pyrano[3,2-b]oxepin

: 440320-43-4
(2R,3S,4S,4aR,9aS)-2-Hydroxymethyl-3,4,4a,6,9,9a-hexahydro-2H-1,5-dioxa-benzocycloheptene-3,4-diol

Guidance literature:: With titanium tetrachloride; In nitromethane; at -5 ℃; for 0.5h;
DOI:10.1016/j.tet.2004.07.010

Reference yield:

: 252046-22-3
(2R,3R,4S,4aS,9aS)-3,4-bis(benzyloxy)-2-(benzyloxymethyl)-2,3,4,4a,9,9a-hexahydro-6H-pyrano[3,2-b]oxepin

: 440320-43-4
(2R,3S,4S,4aR,9aS)-2-Hydroxymethyl-3,4,4a,6,9,9a-hexahydro-2H-1,5-dioxa-benzocycloheptene-3,4-diol

: (2S,3R,4R,5S,6R)-2-((Z)-But-2-enyl)-6-hydroxymethyl-tetrahydro-pyran-3,4,5-triol

Guidance literature:: With ammonia; sodium; In tetrahydrofuran; ethanol; at -78 ℃; for 2h; Title compound not separated from byproducts;
DOI:10.1016/S0040-4020(02)00041-8