Technology Process of C29H50O3
There total 4 articles about C29H50O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: di-isopropyl azodicarboxylate; triphenylphosphine / toluene / 1 h / 20 °C
2: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; acetone / 20 h / 20 °C
3: sodium periodate / water; acetone / 2 h / 20 °C
With
sodium periodate; osmium(VIII) oxide; di-isopropyl azodicarboxylate; 4-methylmorpholine N-oxide; triphenylphosphine;
In
water; acetone; toluene;
1: Mitsunobu reaction;
DOI:10.1002/cbic.201000511
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: N-Bromosuccinimide; triphenylphosphine / dichloromethane / 0.33 h / 4 - 8 °C
2.1: magnesium / tetrahydrofuran / 4.5 h / 20 - 50 °C
2.2: 2 h / -70 - 20 °C
3.1: di-isopropyl azodicarboxylate; triphenylphosphine / toluene / 1 h / 20 °C
4.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; acetone / 20 h / 20 °C
5.1: sodium periodate / water; acetone / 2 h / 20 °C
With
sodium periodate; N-Bromosuccinimide; osmium(VIII) oxide; di-isopropyl azodicarboxylate; magnesium; 4-methylmorpholine N-oxide; triphenylphosphine;
In
tetrahydrofuran; dichloromethane; water; acetone; toluene;
3.1: Mitsunobu reaction;
DOI:10.1002/cbic.201000511