methylphosphinic acid ammonium salt

Base Information

Chemical Name:methylphosphinic acid ammonium salt
CAS No.:80953-54-4
Molecular Formula:C₈H₁₁O₃P*H₃N
Molecular Weight:203.178
Hs Code.:

methyl<o-(hydroxymethyl)phenyl>phosphinic acid ammonium salt

Synonyms:methylphosphinic acid ammonium salt

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Chemical Property of methylphosphinic acid ammonium salt

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Technology Process of methylphosphinic acid ammonium salt

There total 8 articles about methylphosphinic acid ammonium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 75777-30-9
1-methyl-1,3-dihydro-2,1-benzoxaphosphole 1-oxide

: 80953-54-4
methylphosphinic acid ammonium salt

Guidance literature:: With ammonium hydroxide; In water; Heating;
DOI:10.1021/jo00348a013

Reference yield:

: 5159-41-1
2-iodobenzyl alcohol

: 80953-54-4
methylphosphinic acid ammonium salt

Guidance literature:: Multi-step reaction with 4 steps

1: 2 h / Heating

2: 81 percent / NiCl₂ / 0.5 h / 165 - 175 °C

3: 82 percent / 10percent HClO₄ / H₂O / 0.5 h / Heating

4: 91 percent / NH₄OH / H₂O / Heating

With ammonium hydroxide; perchloric acid; nickel dichloride; In water;
DOI:10.1021/jo00348a013

Reference yield:

: 61820-24-4
methyl o-tolylphosphinic acid

: 80953-54-4
methylphosphinic acid ammonium salt

Guidance literature:: Multi-step reaction with 3 steps

1: Cl₂ / CHCl₃ / Heating; Irradiation

2: 66 percent / 10percent HClO₄ / H₂O / 0.5 h / 100 °C

3: 91 percent / NH₄OH / H₂O / Heating

With ammonium hydroxide; perchloric acid; chlorine; In chloroform; water;
DOI:10.1021/jo00348a013