N-((hex-5-ynylimino)methylene)-3-(2-(trimethylsilyl)ethynyl)benzenamine

Base Information

Chemical Name:N-((hex-5-ynylimino)methylene)-3-(2-(trimethylsilyl)ethynyl)benzenamine
CAS No.:1402828-96-9
Molecular Formula:C₁₈H₂₂N₂Si
Molecular Weight:294.472
Hs Code.:

Synonyms:N-((hex-5-ynylimino)methylene)-3-(2-(trimethylsilyl)ethynyl)benzenamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-((hex-5-ynylimino)methylene)-3-(2-(trimethylsilyl)ethynyl)benzenamine

Chemical Property:

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Technology Process of N-((hex-5-ynylimino)methylene)-3-(2-(trimethylsilyl)ethynyl)benzenamine

There total 5 articles about N-((hex-5-ynylimino)methylene)-3-(2-(trimethylsilyl)ethynyl)benzenamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1402828-95-8
1-(hex-5-ynyl)-3-(3-(2-(trimethylsilyl)ethynyl)phenyl)thiourea

: 1402828-96-9
N-((hex-5-ynylimino)methylene)-3-(2-(trimethylsilyl)ethynyl)benzenamine

Guidance literature:: With triethylamine; dibromotriphenylphosphorane; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ma301639m DOI:10.1021/ma301639m

Reference yield:

: 626-01-7
3-Iodoaniline

: 1402828-96-9
N-((hex-5-ynylimino)methylene)-3-(2-(trimethylsilyl)ethynyl)benzenamine

Guidance literature:: Multi-step reaction with 4 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(l) iodide; triphenylphosphine / 36 h / 80 °C / Inert atmosphere

2: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

3: dichloromethane / 1 h / 0 - 20 °C

4: dibromotriphenylphosphorane; triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; triphenylphosphine; dibromotriphenylphosphorane; In dichloromethane; 1: |Sonogashira Cross-Coupling;
DOI:10.1021/ma301639m DOI:10.1021/ma301639m

Reference yield:

: 1066-54-2
trimethylsilylacetylene

: 1402828-96-9
N-((hex-5-ynylimino)methylene)-3-(2-(trimethylsilyl)ethynyl)benzenamine

Guidance literature:: Multi-step reaction with 4 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(l) iodide; triphenylphosphine / 36 h / 80 °C / Inert atmosphere

2: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

3: dichloromethane / 1 h / 0 - 20 °C

4: dibromotriphenylphosphorane; triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; triphenylphosphine; dibromotriphenylphosphorane; In dichloromethane; 1: |Sonogashira Cross-Coupling;
DOI:10.1021/ma301639m DOI:10.1021/ma301639m