Technology Process of C19H30N4O3S
There total 5 articles about C19H30N4O3S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogenchloride;
In
ethanol; water;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 1 h / 0 °C
1.2: 18 h / 0 - 20 °C
2.1: hydrogen / palladium 10% on activated carbon / methanol / 18 h
3.1: dicyclohexyl-carbodiimide; benzotriazol-1-ol / dichloromethane / 0 - 20 °C
4.1: water; lithium hydroxide monohydrate / methanol
5.1: hydrogenchloride / ethanol; water
With
hydrogenchloride; lithium hydroxide monohydrate; water; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide;
palladium 10% on activated carbon;
In
methanol; ethanol; dichloromethane; water;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: hydrogen / palladium 10% on activated carbon / methanol / 18 h
2: dicyclohexyl-carbodiimide; benzotriazol-1-ol / dichloromethane / 0 - 20 °C
3: water; lithium hydroxide monohydrate / methanol
4: hydrogenchloride / ethanol; water
With
hydrogenchloride; lithium hydroxide monohydrate; water; hydrogen; benzotriazol-1-ol; dicyclohexyl-carbodiimide;
palladium 10% on activated carbon;
In
methanol; ethanol; dichloromethane; water;