C₁₇H₂₂INO₃

Base Information

Chemical Name:C₁₇H₂₂INO₃
CAS No.:1393603-61-6
Molecular Formula:C₁₇H₂₂INO₃
Molecular Weight:415.271
Hs Code.:

C<sub>17</sub>H<sub>22</sub>INO<sub>3</sub>

Synonyms:C₁₇H₂₂INO₃

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Chemical Property of C₁₇H₂₂INO₃

Chemical Property:

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Technology Process of C₁₇H₂₂INO₃

There total 7 articles about C₁₇H₂₂INO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1484-84-0
2(RS)-(2-hydroxyethyl)piperidine

: 1393603-61-6
C₁₇H₂₂INO₃

Guidance literature:: Multi-step reaction with 8 steps

1.1: tetrahydrofuran; methanol / 0.5 h / 35 - 55 °C / Resolution of racemate

2.1: triethylamine / dichloromethane / 20 °C

3.1: phosgene; dimethyl sulfoxide / dichloromethane / 0.33 h / -78 °C / Inert atmosphere

3.2: 4 h / 20 °C / Inert atmosphere

4.1: tetrahydrofuran; diethyl ether / 4.5 h / -78 - 20 °C / Inert atmosphere

5.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 2 h / 20 °C

6.1: sodium hydroxide / methanol / 16 h / 55 °C

7.1: trifluoroacetic acid / dichloromethane / 1 h / 0 °C

8.1: sodium hydroxide / tetrahydrofuran / 4 h / 0 - 20 °C

With phosgene; sodium hydrogencarbonate; Dess-Martin periodane; dimethyl sulfoxide; triethylamine; trifluoroacetic acid; sodium hydroxide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; 3.1: Swern oxidation / 3.2: Swern oxidation;
DOI:10.1039/c2ob25880c

Reference yield:

: 1214914-34-7
(S)-2-(2-oxo-propyl)-piperidine-1-carboxylic acid tert-butyl ester

: 1393603-61-6
C₁₇H₂₂INO₃

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide / methanol / 16 h / 55 °C

2: trifluoroacetic acid / dichloromethane / 1 h / 0 °C

3: sodium hydroxide / tetrahydrofuran / 4 h / 0 - 20 °C

With trifluoroacetic acid; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1039/c2ob25880c

Reference yield:

: 1393603-60-5
(S,E)-tert-butyl-2-(4-(2-iodo-4,5-dimethoxyphenyl)-2-oxobut-3-enyl)piperidine-1-carboxylate

: 1393603-61-6
C₁₇H₂₂INO₃

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / 1 h / 0 °C

2: sodium hydroxide / tetrahydrofuran / 4 h / 0 - 20 °C

With trifluoroacetic acid; sodium hydroxide; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c2ob25880c