Technology Process of C63H102O28
There total 6 articles about C63H102O28 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium hydroxide;
In
tetrahydrofuran; water;
for 2h;
Inert atmosphere;
Reflux;
DOI:10.1039/b9nj00305c
- Guidance literature:
-
Multi-step reaction with 5 steps
1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 12 h / 80 °C
2: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / 60 °C
3: thionyl chloride / dichloromethane / 3 h / 20 °C
4: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 12 h / 80 °C
5: potassium hydroxide / tetrahydrofuran; water; methanol / 4 h / 50 °C
With
lithium aluminium tetrahydride; thionyl chloride; potassium carbonate; potassium iodide; potassium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
1: |Williamson Ether Synthesis / 4: |Williamson Ether Synthesis;
DOI:10.1021/acs.chemmater.7b02928
- Guidance literature:
-
Multi-step reaction with 4 steps
1: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / 60 °C
2: thionyl chloride / dichloromethane / 3 h / 20 °C
3: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 12 h / 80 °C
4: potassium hydroxide / tetrahydrofuran; water; methanol / 4 h / 50 °C
With
lithium aluminium tetrahydride; thionyl chloride; potassium carbonate; potassium iodide; potassium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
3: |Williamson Ether Synthesis;
DOI:10.1021/acs.chemmater.7b02928