3,3-dimethyl-5-(2-(1-trityl-1H-imidazol-4-yl)phenoxy)pentyl 4-methylbenzene sulfonate

Base Information

Chemical Name:3,3-dimethyl-5-(2-(1-trityl-1H-imidazol-4-yl)phenoxy)pentyl 4-methylbenzene sulfonate
CAS No.:1192813-82-3
Molecular Formula:C₄₂H₄₂N₂O₄S
Molecular Weight:670.872
Hs Code.:

Synonyms:3,3-dimethyl-5-(2-(1-trityl-1H-imidazol-4-yl)phenoxy)pentyl 4-methylbenzene sulfonate

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Chemical Property of 3,3-dimethyl-5-(2-(1-trityl-1H-imidazol-4-yl)phenoxy)pentyl 4-methylbenzene sulfonate

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Technology Process of 3,3-dimethyl-5-(2-(1-trityl-1H-imidazol-4-yl)phenoxy)pentyl 4-methylbenzene sulfonate

There total 1 articles about 3,3-dimethyl-5-(2-(1-trityl-1H-imidazol-4-yl)phenoxy)pentyl 4-methylbenzene sulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1192815-25-0
2-(1-trityl-1H-imidazol-4-yl)phenol

: 53120-76-6
3,3-dimethylpentane-1,5-diyl bis(4-methylbenzenesulfonate)

: 1192813-82-3
3,3-dimethyl-5-(2-(1-trityl-1H-imidazol-4-yl)phenoxy)pentyl 4-methylbenzene sulfonate

: 5,5'-(2,2'-(3,3-dimethylpentane-1,5-diyl)bis(oxy)bis(2,1-phenylene))bis(1H-imidazole)

Guidance literature:: 2-(1-trityl-1H-imidazol-4-yl)phenol; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 0.25h;

3,3-dimethylpentane-1,5-diyl bis(4-methylbenzenesulfonate); In N,N-dimethyl-formamide; at 20 ℃;

Reference yield: 8.0%

: 504-29-0
2-aminopyridine

: 1192813-82-3
3,3-dimethyl-5-(2-(1-trityl-1H-imidazol-4-yl)phenoxy)pentyl 4-methylbenzene sulfonate

: N-(5-(2-(1H-imidazol-5-yl)phenoxy)-3,3-dimethylpentyl)pyridin-2-amine

Guidance literature:: 2-aminopyridine; With sodium hydride; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 0.25h;

3,3-dimethyl-5-(2-(1-trityl-1H-imidazol-4-yl)phenoxy)pentyl 4-methylbenzene sulfonate; In N,N-dimethyl-formamide; at 80 ℃;

With acetic acid; In methanol; at 80 ℃; for 3h;

Reference yield:

: 1192813-82-3
3,3-dimethyl-5-(2-(1-trityl-1H-imidazol-4-yl)phenoxy)pentyl 4-methylbenzene sulfonate

: 1300729-48-9
5-chloro-3-(1H-imidazol-5-yl)benzene-1,2-diol

Guidance literature:: 3,3-dimethyl-5-(2-(1-trityl-1H-imidazol-4-yl)phenoxy)pentyl 4-methylbenzene sulfonate; With sodium hydride; benzo[1,3]dioxolo-5-ylamine; In N,N-dimethyl-formamide; at 20 - 80 ℃;

With acetic acid; In methanol; N,N-dimethyl-formamide;

With sodium hydrogencarbonate; In methanol; dichloromethane; water; N,N-dimethyl-formamide;