[(ReOCl(N-(N'',N''-diethylaminothiocarbonyl)-N'-picolylbenzamidine(-2H)))2O]

Base Information

Chemical Name:[(ReOCl(N-(N'',N''-diethylaminothiocarbonyl)-N'-picolylbenzamidine(-2H)))2O]
CAS No.:1031794-96-3
Molecular Formula:C₃₆H₄₂Cl₂N₈O₃Re₂S₂
Molecular Weight:1142.23
Hs Code.:

Synonyms:[(ReOCl(N-(N'',N''-diethylaminothiocarbonyl)-N'-picolylbenzamidine(-2H)))2O]

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Chemical Property of [(ReOCl(N-(N'',N''-diethylaminothiocarbonyl)-N'-picolylbenzamidine(-2H)))2O]

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Technology Process of [(ReOCl(N-(N'',N''-diethylaminothiocarbonyl)-N'-picolylbenzamidine(-2H)))2O]

There total 2 articles about [(ReOCl(N-(N'',N''-diethylaminothiocarbonyl)-N'-picolylbenzamidine(-2H)))2O] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: [ReOCl₃(PPh₃)₂]

: 1031794-91-8
N-(N'',N''-diethylaminothiocarbonyl)-N'-picolylbenzamidine

: 1031794-96-3
[(ReOCl(N-(N'',N''-diethylaminothiocarbonyl)-N'-picolylbenzamidine(-2H)))2O]

Guidance literature:: With (C₂H₅)3N; In dichloromethane; acetone; byproducts: (C2H5)3NHCl; SC(N(C2H5)2)NC(C6H5)NHCH2C5H4N in acetone and (C2H5)3N added to a suspn.of Re complex in CH2Cl2, refluxed for 30 min; evapd. (vac.), washed (MeOH), recrystd. (CH2Cl2/acetone);
DOI:10.1021/ic702344s

Reference yield: 40.0%

: tetra-n-butylammonium tetrachlorooxorhenate(V)

: 1031794-91-8
N-(N'',N''-diethylaminothiocarbonyl)-N'-picolylbenzamidine

: 1031794-96-3
[(ReOCl(N-(N'',N''-diethylaminothiocarbonyl)-N'-picolylbenzamidine(-2H)))2O]

Guidance literature:: With (C₂H₅)3N; In acetone; byproducts: (C2H5)3NHCl; a soln. of SC(N(C2H5)2)NC(C6H5)NHCH2C5H4N and (C2H5)3N in acetone added dropwise to a soln. of Re complex in acetone, stirred at ambient temp. for 2 h; solvent-removed, washed (H2O), extd. (CH2Cl2), recrystd. (CH2Cl2/acetone); elem. anal.;
DOI:10.1021/ic702344s