Technology Process of 4-Hydroxy-5,6,7,8-tetrahydronaphthalene-1,2-dione
There total 12 articles about 4-Hydroxy-5,6,7,8-tetrahydronaphthalene-1,2-dione which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
5,6,7,8-Tetrahydro-2-naphthol;
With
tetrakis(actonitrile)copper(I) hexafluorophosphate; N,N'-di-tert-butylethylenediamine; oxygen;
In
dichloromethane;
at 20 - 23 ℃;
for 4h;
under 760.051 Torr;
With
sulfuric acid; water;
In
dichloromethane;
at 0 - 20 ℃;
for 1.08333h;
Inert atmosphere;
DOI:10.1016/j.tet.2015.04.095
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sulfuric acid / 30 °C
2: ethanol; aqueous HCl / Behandeln des Reaktionsgemisches mit K2Cr2O7 und wss.H2SO4
With
hydrogenchloride; ethanol; sulfuric acid;
DOI:10.1111/j.1751-0813.2000.tb11742.x