(1R,2R)-N₁-{6-(trifluoromethyl)-1H-benzo[d]imidazol-2-yl}cyclohexane-1,2-diamine

Base Information

• Chemical Name: (1R,2R)-N₁-{6-(trifluoromethyl)-1H-benzo[d]imidazol-2-yl}cyclohexane-1,2-diamine
• CAS No.: 1170773-36-0
• Molecular Formula: C₁₄H₁₇F₃N₄
• Molecular Weight: 298.311

Synonyms:(1R,2R)-N₁-{6-(trifluoromethyl)-1H-benzo[d]imidazol-2-yl}cyclohexane-1,2-diamine

Chemical Property of (1R,2R)-N₁-{6-(trifluoromethyl)-1H-benzo[d]imidazol-2-yl}cyclohexane-1,2-diamine

Chemical Property:

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Technology Process of (1R,2R)-N₁-{6-(trifluoromethyl)-1H-benzo[d]imidazol-2-yl}cyclohexane-1,2-diamine

There total 1 articles about (1R,2R)-N₁-{6-(trifluoromethyl)-1H-benzo[d]imidazol-2-yl}cyclohexane-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

2-chloro-6-(trifluoromethyl)-1H-benzo[d]imidazole (86604-86-6) + (1R,2R)-1,2-diaminocyclohexane (20439-47-8) → (1R,2R)-N1-{6-(trifluoromethyl)-1H-benzo[d]imidazol-2-yl}cyclohexane-1,2-diamine (1170773-36-0) + C22H20F6N6

Guidance literature:

With triethylamine; at 195 - 200 ℃; for 16h; Inert atmosphere;

DOI:10.1021/jo9010552

Reference yield: 75.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + (1R,2R)-N1-{6-(trifluoromethyl)-1H-benzo[d]imidazol-2-yl}cyclohexane-1,2-diamine (1170773-36-0) → (1R,2R)-N1,N1-dimethyl-N2-{6-(trifluromethyl)-1H-benzo[d]imidazol-2-yl}cyclohexane-1,2-diamine (1170773-35-9)

Guidance literature:

With formic acid; water; at 120 ℃; for 16h;

DOI:10.1021/jo9010552

upstream raw materials:

2-chloro-6-(trifluoromethyl)-1H-benzo[d]imidazole

(1R,2R)-1,2-diaminocyclohexane

Downstream raw materials:

(1R,2R)-N₁,N₁-dimethyl-N₂-{6-(trifluromethyl)-1H-benzo[d]imidazol-2-yl}cyclohexane-1,2-diamine

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