N-cyclohexyl-N'-(3-methoxyphenyl)methanediimine

Base Information

• Chemical Name: N-cyclohexyl-N'-(3-methoxyphenyl)methanediimine
• CAS No.: 122077-94-5
• Molecular Formula: C₁₄H₁₈N₂O
• Molecular Weight: 230.31
• Mol file: 122077-94-5.mol

Synonyms:N-cyclohexyl-N'-(3-methoxyphenyl)methanediimine

Chemical Property of N-cyclohexyl-N'-(3-methoxyphenyl)methanediimine

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of N-cyclohexyl-N'-(3-methoxyphenyl)methanediimine

There total 1 articles about N-cyclohexyl-N'-(3-methoxyphenyl)methanediimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

Cyclohexyl isocyanide (931-53-3) + m-Anisidine (536-90-3,918666-97-4) → N-cyclohexyl-N'-(3-methoxyphenyl)methanediimine (122077-94-5)

Guidance literature:

With tetra-(n-butyl)ammonium iodide; In acetonitrile; at 50 ℃; for 12h; Inert atmosphere; Electrochemical reaction;

DOI:10.1021/acs.orglett.0c00510

Reference yield: 70.0%

2-methyl-4,4-diphenylbuta-2,3-dienoic acid (6002-06-8) + N-cyclohexyl-N'-(3-methoxyphenyl)methanediimine (122077-94-5) → (1RS,7SR)-N-cyclohexyl-8-methoxy-4-methyl-3-oxo-6,6-diphenyl-2-azatricyclo<5.2.2.01,5>undeca-4,8,10-triene-2-carboxamide (136472-44-1)

Guidance literature:

DOI:10.1002/hlca.19910740512

Reference yield: 12.0%

2-methyl-4-phenyl-2,3-allenoic acid (57496-47-6) + N-cyclohexyl-N'-(3-methoxyphenyl)methanediimine (122077-94-5) → (1RS,6RS,7SR)-2-(N-cyclohexylcarbamoyl)-8-methoxy-4-methyl-6-phenyl-2-azatricyclo<5.2.2.01,5>undeca-4,8,10-trien-3-one + (1RS,6SR,7SR)-2-(N-cyclohexylcarbamoyl)-8-methoxy-4-methyl-6-phenyl-2-azatricyclo<5.2.2.01,5>undeca-4,8,10-trien-3-one

Guidance literature:

In tetrahydrofuran; for 48h; Mechanism; Ambient temperature; other carbodiimides;

DOI:10.1002/hlca.19890720108

upstream raw materials:

Cyclohexyl isocyanide

m-Anisidine

Downstream raw materials:

(1RS,7SR)-N-cyclohexyl-8-methoxy-4-methyl-3-oxo-6,6-diphenyl-2-azatricyclo<5.2.2.0^1,5>undeca-4,8,10-triene-2-carboxamide