tris{2,6-dimethoxy-4-[2-(E)-[4-(dimethylamino)phenyl]ethenyl]phenyl}methanol

Base Information

Chemical Name:tris{2,6-dimethoxy-4-[2-(E)-[4-(dimethylamino)phenyl]ethenyl]phenyl}methanol
CAS No.:897963-70-1
Molecular Formula:C₅₅H₆₁N₃O₇
Molecular Weight:876.105
Hs Code.:

Synonyms:tris{2,6-dimethoxy-4-[2-(E)-[4-(dimethylamino)phenyl]ethenyl]phenyl}methanol

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Chemical Property of tris{2,6-dimethoxy-4-[2-(E)-[4-(dimethylamino)phenyl]ethenyl]phenyl}methanol

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Technology Process of tris{2,6-dimethoxy-4-[2-(E)-[4-(dimethylamino)phenyl]ethenyl]phenyl}methanol

There total 4 articles about tris{2,6-dimethoxy-4-[2-(E)-[4-(dimethylamino)phenyl]ethenyl]phenyl}methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: N,N-dimethyl-4-[(E)-2-(3,5-dimethoxyphenyl)ethenyl]phenylamine

: 105-58-8,76619-83-5
Diethyl carbonate

: 897963-70-1
tris{2,6-dimethoxy-4-[2-(E)-[4-(dimethylamino)phenyl]ethenyl]phenyl}methanol

Guidance literature:: N,N-dimethyl-4-[(E)-2-(3,5-dimethoxyphenyl)ethenyl]phenylamine; With n-butyllithium; In diethyl ether; at 20 ℃; for 20h;

Diethyl carbonate; In diethyl ether; at 0 - 40 ℃; for 48h;
DOI:10.1016/j.jorganchem.2006.02.017

Reference yield:

: 705-76-0
3,5-dimethoxybenzyl alcohol

: 897963-70-1
tris{2,6-dimethoxy-4-[2-(E)-[4-(dimethylamino)phenyl]ethenyl]phenyl}methanol

Guidance literature:: Multi-step reaction with 3 steps

1.1: 89.5 percent / iodine / 3 h / 150 °C

2.1: sodium hydride / tetrahydrofuran / 1 h / 20 °C

2.2: 67.5 percent / tetrahydrofuran / 18 h / Heating

3.1: nBuLi / diethyl ether; various solvent(s) / 20 h / 20 °C

3.2: 52 percent / diethyl ether; various solvent(s) / 48 h / 0 - 40 °C

With n-butyllithium; iodine; sodium hydride; In tetrahydrofuran; diethyl ether;
DOI:10.1016/j.jorganchem.2006.02.017

Reference yield:

: 100-10-7
4-dimethylamino-benzaldehyde

: 897963-70-1
tris{2,6-dimethoxy-4-[2-(E)-[4-(dimethylamino)phenyl]ethenyl]phenyl}methanol

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran / 1 h / 20 °C

1.2: 67.5 percent / tetrahydrofuran / 18 h / Heating

2.1: nBuLi / diethyl ether; various solvent(s) / 20 h / 20 °C

2.2: 52 percent / diethyl ether; various solvent(s) / 48 h / 0 - 40 °C

With n-butyllithium; sodium hydride; In tetrahydrofuran; diethyl ether;
DOI:10.1016/j.jorganchem.2006.02.017