N-BOC-L-pipecolyl-L-p-nitrophenylalanine tert-butyl ester

Base Information

Chemical Name:N-BOC-L-pipecolyl-L-p-nitrophenylalanine tert-butyl ester
CAS No.:145037-70-3
Molecular Formula:C₂₄H₃₅N₃O₇
Molecular Weight:477.558
Hs Code.:

Synonyms:N-BOC-L-pipecolyl-L-p-nitrophenylalanine tert-butyl ester

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Chemical Property of N-BOC-L-pipecolyl-L-p-nitrophenylalanine tert-butyl ester

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Technology Process of N-BOC-L-pipecolyl-L-p-nitrophenylalanine tert-butyl ester

There total 1 articles about N-BOC-L-pipecolyl-L-p-nitrophenylalanine tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 26250-84-0
(S)-(-)-1-(tert-butoxycarbonyl)-2-piperidinecarboxylic acid

: 116366-32-6
L-4-nitrophenylalanine tert-butyl ester

: 145037-70-3
N-BOC-L-pipecolyl-L-p-nitrophenylalanine tert-butyl ester

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 0 - 20 ℃; for 2h;
DOI:10.1021/jm00101a005

Reference yield: 69.0%

: 145037-70-3
N-BOC-L-pipecolyl-L-p-nitrophenylalanine tert-butyl ester

: 145037-71-4
L-pipecolyl-L-p-nitrophenylalanine tert-butyl ester

Guidance literature:: With hydrogenchloride; In ethyl acetate; for 3h;
DOI:10.1021/jm00101a005

Reference yield:

: 145037-70-3
N-BOC-L-pipecolyl-L-p-nitrophenylalanine tert-butyl ester

: (S)-2-({(S)-1-[2-(3-Methoxy-phenyl)-2-oxo-ethyl]-piperidine-2-carbonyl}-amino)-3-(4-nitro-phenyl)-propionic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent / HCl / ethyl acetate / 3 h

2: 57 percent / potassium fluoride on Celite / acetonitrile / Ambient temperature

With hydrogenchloride; potassium fluoride on Celite; In ethyl acetate; acetonitrile;
DOI:10.1021/jm00101a005