N--(S)-valine methyl ester

Base Information

Chemical Name:N--(S)-valine methyl ester
CAS No.:55325-57-0
Molecular Formula:C₁₇H₂₄N₂O₆
Molecular Weight:352.387
Hs Code.:

N-<N'-(benzyloxycarbonyl)-(S)-seryl>-(S)-valine methyl ester

Synonyms:N--(S)-valine methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N--(S)-valine methyl ester

Chemical Property:

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Technology Process of N--(S)-valine methyl ester

There total 4 articles about N--(S)-valine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1145-80-8
N-(benzyloxycarbonyl)-L-serine

: 6306-52-1
L-valine methylester hydrochloride

: 55325-57-0
N--(S)-valine methyl ester

Guidance literature:: L-valine methylester hydrochloride; With sodium carbonate; In dichloromethane; water; at 20 ℃; for 0.0833333h;

N-(benzyloxycarbonyl)-L-serine; With C₁₂H₆B₂Br₄O₃; In 1,2-dichloro-ethane; at 90 ℃; for 24h; chemoselective reaction;
DOI:10.1021/acs.orglett.0c03252

Reference yield: 60.0%

: N-<(S)-3'-(benzyloxycarbonyl)-1',3'-oxazolidine-4'-carbonyl>-(S)-valine methyl ester

: 55325-57-0
N--(S)-valine methyl ester

Guidance literature:: With hydrogenchloride; methanol; for 12h; Ambient temperature;
DOI:10.1016/0957-4166(94)00386-P

Reference yield:

: 62631-10-1
N-benzyloxycarbonyl-D-serine hydrazide

: 55325-57-0
N-(N-benzyloxycarbonyl-D-seryl)-D-valine methyl ester

Guidance literature:: With hydrogenchloride; acetic acid; sodium nitrite; Behandeln einer Loesung des Reaktionsprodukts in Aethylacetat mit D-Valin-methylester;
DOI:10.1021/ja01630a040