Technology Process of C42H52N8O17
There total 10 articles about C42H52N8O17 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
lithium hydroxide;
In
tetrahydrofuran; water;
at 0 ℃;
for 1h;
DOI:10.1021/ol2022356
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: lithium hydroxide / tetrahydrofuran; water / 1 h / 0 °C
2.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 1 h / 0 °C
2.2: 24 h / 20 °C / Inert atmosphere
3.1: lithium hydroxide / tetrahydrofuran; water / 1 h / 0 °C
With
benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; lithium hydroxide;
In
tetrahydrofuran; dichloromethane; water;
DOI:10.1021/ol2022356
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: dimethyl 1-(1-diazo-2-oxopropyl)phosphonate / methanol / 0.08 h / 0 °C
1.2: 12 h / 20 °C
2.1: copper(II) sulfate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine / water; tert-butyl alcohol
2.2: 16 h
3.1: lithium hydroxide / tetrahydrofuran; water / 1 h / 0 °C
4.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 1 h / 0 °C
4.2: 24 h / 20 °C / Inert atmosphere
5.1: lithium hydroxide / tetrahydrofuran; water / 1 h / 0 °C
With
dimethyl 1-(1-diazo-2-oxopropyl)phosphonate; benzotriazol-1-ol; copper(II) sulfate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; lithium hydroxide; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine;
In
tetrahydrofuran; methanol; dichloromethane; water; tert-butyl alcohol;
DOI:10.1021/ol2022356
