2-C-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-7-mesyloxy-1,3,6-trimethoxyxanthone

Base Information

• Chemical Name: 2-C-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-7-mesyloxy-1,3,6-trimethoxyxanthone
• CAS No.: 1239694-39-3
• Molecular Formula: C₅₁H₅₀O₁₃S
• Molecular Weight: 903.016

Synonyms:2-C-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-7-mesyloxy-1,3,6-trimethoxyxanthone

Chemical Property of 2-C-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-7-mesyloxy-1,3,6-trimethoxyxanthone

Chemical Property:

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Technology Process of 2-C-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-7-mesyloxy-1,3,6-trimethoxyxanthone

There total 1 articles about 2-C-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-7-mesyloxy-1,3,6-trimethoxyxanthone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

2-C-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-7-mesyloxy-1,3,6-trimethoxyxanthene (1239694-36-0) → 2-C-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-7-mesyloxy-1,3,6-trimethoxyxanthone (1239694-39-3)

Guidance literature:

2-C-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-7-mesyloxy-1,3,6-trimethoxyxanthene; With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In 1,4-dioxane; dichloromethane; water; at 0 - 20 ℃;

With dmap; In 1,4-dioxane; dichloromethane; water; ethyl acetate;

DOI:10.1021/jo100776q

Reference yield: 88.0%

2-C-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-7-mesyloxy-1,3,6-trimethoxyxanthone (1239694-39-3)

Guidance literature:

With sodium hydroxide; In 1,4-dioxane; water; at 60 ℃; for 24h;

DOI:10.1021/jo100776q

upstream raw materials:

2-C-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-7-mesyloxy-1,3,6-trimethoxyxanthene

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