5-(4-{[1-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-1H-1,2,3-triazol-4-yl]methoxy}phenyl)-3-(4-bromophenyl)-1,2,4-oxadiazole

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Chemical Name:5-(4-{[1-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-1H-1,2,3-triazol-4-yl]methoxy}phenyl)-3-(4-bromophenyl)-1,2,4-oxadiazole
CAS No.:957470-99-4
Molecular Formula:C₃₁H₃₀BrN₅O₁₁
Molecular Weight:728.51
Hs Code.:

Synonyms:5-(4-{[1-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-1H-1,2,3-triazol-4-yl]methoxy}phenyl)-3-(4-bromophenyl)-1,2,4-oxadiazole

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Chemical Property of 5-(4-{[1-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-1H-1,2,3-triazol-4-yl]methoxy}phenyl)-3-(4-bromophenyl)-1,2,4-oxadiazole

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Technology Process of 5-(4-{[1-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-1H-1,2,3-triazol-4-yl]methoxy}phenyl)-3-(4-bromophenyl)-1,2,4-oxadiazole

There total 3 articles about 5-(4-{[1-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-1H-1,2,3-triazol-4-yl]methoxy}phenyl)-3-(4-bromophenyl)-1,2,4-oxadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 957470-91-6
3-(4-bromophenyl)-5-[4-(prop-2-yn-1-yloxy)phenyl]-1,2,4-oxadiazole

: 13992-25-1
1-azido-1-deoxy-β-D-glucopyranoside tetraacetate

: 957470-99-4
5-(4-{[1-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-1H-1,2,3-triazol-4-yl]methoxy}phenyl)-3-(4-bromophenyl)-1,2,4-oxadiazole

Guidance literature:: With copper diacetate; sodium L-ascorbate; In dichloromethane; water; at 20 ℃; for 20h;
DOI:10.1016/j.carres.2007.07.011

Reference yield:

: 422536-00-3
3-(4-bromophenyl)-5-(4-hydroxyphenyl)-1,2,4-oxadiazole

: 957470-99-4
5-(4-{[1-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-1H-1,2,3-triazol-4-yl]methoxy}phenyl)-3-(4-bromophenyl)-1,2,4-oxadiazole

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / K₂CO₃ / dimethylformamide; toluene / 30 h / 20 °C

2: 60 percent / Cu(OAc)2; sodium ascorbate / CH₂Cl₂; H₂O / 20 h / 20 °C

With copper diacetate; potassium carbonate; sodium L-ascorbate; In dichloromethane; water; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.carres.2007.07.011

Reference yield:

: 331989-76-5
3-(4-bromophenyl)-5-(4-methoxyphenyl)-1,2,4-oxadiazole

: 957470-99-4
5-(4-{[1-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-1H-1,2,3-triazol-4-yl]methoxy}phenyl)-3-(4-bromophenyl)-1,2,4-oxadiazole

Guidance literature:: Multi-step reaction with 3 steps

1: 64 percent / BBr₃ / CH₂Cl₂ / 20 h / Heating

2: 76 percent / K₂CO₃ / dimethylformamide; toluene / 30 h / 20 °C

3: 60 percent / Cu(OAc)2; sodium ascorbate / CH₂Cl₂; H₂O / 20 h / 20 °C

With copper diacetate; boron tribromide; potassium carbonate; sodium L-ascorbate; In dichloromethane; water; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.carres.2007.07.011