hydrazino-4-(5-methylsulfanyl-1,3,4-oxadiazol-2-yl)anilinomethanethione

Base Information

Chemical Name:hydrazino-4-(5-methylsulfanyl-1,3,4-oxadiazol-2-yl)anilinomethanethione
CAS No.:328118-02-1
Molecular Formula:C₁₀H₁₁N₅OS₂
Molecular Weight:281.362
Hs Code.:

Synonyms:hydrazino-4-(5-methylsulfanyl-1,3,4-oxadiazol-2-yl)anilinomethanethione

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of hydrazino-4-(5-methylsulfanyl-1,3,4-oxadiazol-2-yl)anilinomethanethione

Chemical Property:

Purity/Quality:

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Technology Process of hydrazino-4-(5-methylsulfanyl-1,3,4-oxadiazol-2-yl)anilinomethanethione

There total 3 articles about hydrazino-4-(5-methylsulfanyl-1,3,4-oxadiazol-2-yl)anilinomethanethione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1350301-74-4
5-(4-isothiocyanatophenyl)-2-methylsulfanyl-1,3,4-oxadiazole

: 328118-02-1
hydrazino-4-(5-methylsulfanyl-1,3,4-oxadiazol-2-yl)anilinomethanethione

Guidance literature:: 5-(4-isothiocyanatophenyl)-2-methylsulfanyl-1,3,4-oxadiazole; With toluene sulfonyl chloride; In tetrahydrofuran; at 20 ℃; for 1h; Reflux;

With hydrazine hydrate; In tetrahydrofuran; at 20 ℃;

Reference yield:

: 5351-17-7
4-aminobenzohydrazide

: 328118-02-1
hydrazino-4-(5-methylsulfanyl-1,3,4-oxadiazol-2-yl)anilinomethanethione

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium hydroxide; hydrazine hydrate / water; methanol / 24 h / Reflux

2.1: potassium hydroxide / methanol / 4 h / 20 °C

3.1: potassium hydroxide / methanol / 4 h / 20 °C

4.1: toluene sulfonyl chloride / tetrahydrofuran / 1 h / 20 °C / Reflux

4.2: 20 °C

With toluene sulfonyl chloride; hydrazine hydrate; potassium hydroxide; In tetrahydrofuran; methanol; water;

Reference yield:

: 203268-83-1,32058-82-5
5-(4-aminophenyl)-1,3,4-oxadiazole-2-thiol

: 328118-02-1
hydrazino-4-(5-methylsulfanyl-1,3,4-oxadiazol-2-yl)anilinomethanethione

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium hydroxide / methanol / 4 h / 20 °C

2.1: potassium hydroxide / methanol / 4 h / 20 °C

3.1: toluene sulfonyl chloride / tetrahydrofuran / 1 h / 20 °C / Reflux

3.2: 20 °C

With toluene sulfonyl chloride; potassium hydroxide; In tetrahydrofuran; methanol;