3-propenyl 4-[3-(4-(decyloxy)phenoxy)-2-hydroxypropoxy]benzoate

Base Information

• Chemical Name: 3-propenyl 4-[3-(4-(decyloxy)phenoxy)-2-hydroxypropoxy]benzoate
• CAS No.: 408501-45-1
• Molecular Formula: C₂₉H₄₀O₆
• Molecular Weight: 484.633
• Mol file: 408501-45-1.mol

Synonyms:3-propenyl 4-[3-(4-(decyloxy)phenoxy)-2-hydroxypropoxy]benzoate

Chemical Property of 3-propenyl 4-[3-(4-(decyloxy)phenoxy)-2-hydroxypropoxy]benzoate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 3-propenyl 4-[3-(4-(decyloxy)phenoxy)-2-hydroxypropoxy]benzoate

There total 3 articles about 3-propenyl 4-[3-(4-(decyloxy)phenoxy)-2-hydroxypropoxy]benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

allyl 4-hydroxybenzoate (18982-18-8) + 2-[(4-(decyloxy)phenoxy)methyl]oxirane (408501-42-8) → 3-propenyl 4-[3-(4-(decyloxy)phenoxy)-2-hydroxypropoxy]benzoate (408501-45-1)

Guidance literature:

With 1,4-diaza-bicyclo[2.2.2]octane; In N,N-dimethyl-formamide; for 3h; Heating;

DOI:10.1021/jm011050x

Reference yield:

1-bromo dodecane (112-29-8) → 3-propenyl 4-[3-(4-(decyloxy)phenoxy)-2-hydroxypropoxy]benzoate (408501-45-1)

Guidance literature:

Multi-step reaction with 3 steps

1.1: NaH / dimethylformamide / 0.33 h

1.2: 36 percent / dimethylformamide / 3 h

2.1: 91 percent / Cs₂CO₃ / acetonitrile / 3 h / Heating

3.1: 64 percent / DABCO / dimethylformamide / 3 h / Heating

With 1,4-diaza-bicyclo[2.2.2]octane; sodium hydride; caesium carbonate; In N,N-dimethyl-formamide; acetonitrile;

DOI:10.1021/jm011050x

Reference yield:

4-decyloxyphenol (35108-00-0) → 3-propenyl 4-[3-(4-(decyloxy)phenoxy)-2-hydroxypropoxy]benzoate (408501-45-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 91 percent / Cs₂CO₃ / acetonitrile / 3 h / Heating

2: 64 percent / DABCO / dimethylformamide / 3 h / Heating

With 1,4-diaza-bicyclo[2.2.2]octane; caesium carbonate; In N,N-dimethyl-formamide; acetonitrile;

DOI:10.1021/jm011050x

upstream raw materials:

allyl 4-hydroxybenzoate

2-[(4-(decyloxy)phenoxy)methyl]oxirane

1-bromo dodecane

4-decyloxyphenol

Downstream raw materials:

4-[3-(4-decyloxy-phenoxy)-2-oxo-propoxy]-benzoic acid allyl ester