(R)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionic acid (2S,3R)-3-decyl-oxiranylmethyl ester

Base Information

Chemical Name:(R)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionic acid (2S,3R)-3-decyl-oxiranylmethyl ester
CAS No.:874461-82-2
Molecular Formula:C₂₃H₃₃F₃O₄
Molecular Weight:430.508
Hs Code.:

Synonyms:(R)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionic acid (2S,3R)-3-decyl-oxiranylmethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionic acid (2S,3R)-3-decyl-oxiranylmethyl ester

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Technology Process of (R)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionic acid (2S,3R)-3-decyl-oxiranylmethyl ester

There total 4 articles about (R)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionic acid (2S,3R)-3-decyl-oxiranylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 51887-25-3
tridec-2-yn-1-ol

: 874461-82-2
(R)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionic acid (2S,3R)-3-decyl-oxiranylmethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen / Lindlar's catalyst / pyridine / 24 h

2: titanium(IV) isopropylate; tert.-butylhydroperoxide; calcium hydride; diethyl (2R,3R)-tartrate; silica gel / dichloromethane / 21 h / -40 °C

3: pyridine / tetrachloromethane / Ambient temperature

With pyridine; titanium(IV) isopropylate; tert.-butylhydroperoxide; calcium hydride; diethyl (2R,3R)-tartrate; hydrogen; silica gel; Lindlar's catalyst; In pyridine; tetrachloromethane; dichloromethane;
DOI:10.1021/ja00184a035

Reference yield:

: 74962-99-5,68480-25-1
(Z)-tridec-2-en-1-ols

: 874461-82-2
(R)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionic acid (2S,3R)-3-decyl-oxiranylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: titanium(IV) isopropylate; tert.-butylhydroperoxide; calcium hydride; diethyl (2R,3R)-tartrate; silica gel / dichloromethane / 21 h / -40 °C

2: pyridine / tetrachloromethane / Ambient temperature

With pyridine; titanium(IV) isopropylate; tert.-butylhydroperoxide; calcium hydride; diethyl (2R,3R)-tartrate; silica gel; In tetrachloromethane; dichloromethane;
DOI:10.1021/ja00184a035