1-Benzyloxycarbonyl-2-(tert-butoxycarbonyl)-1-isopropyl-2-tosylhydrazine

Base Information

Chemical Name:1-Benzyloxycarbonyl-2-(tert-butoxycarbonyl)-1-isopropyl-2-tosylhydrazine
CAS No.:286373-57-7
Molecular Formula:C₂₃H₃₀N₂O₆S
Molecular Weight:462.567
Hs Code.:

Synonyms:1-Benzyloxycarbonyl-2-(tert-butoxycarbonyl)-1-isopropyl-2-tosylhydrazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Benzyloxycarbonyl-2-(tert-butoxycarbonyl)-1-isopropyl-2-tosylhydrazine

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Technology Process of 1-Benzyloxycarbonyl-2-(tert-butoxycarbonyl)-1-isopropyl-2-tosylhydrazine

There total 1 articles about 1-Benzyloxycarbonyl-2-(tert-butoxycarbonyl)-1-isopropyl-2-tosylhydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 67-63-0,8013-70-5
isopropyl alcohol

: 200813-53-2
1-tert-butoxycarbonyl-1-tosyl-2-benzyloxycarbonylhydrazine

: 286373-57-7
1-Benzyloxycarbonyl-2-(tert-butoxycarbonyl)-1-isopropyl-2-tosylhydrazine

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 20 ℃;
DOI:10.1039/b000139m

Reference yield: 96.0%

: 286373-57-7
1-Benzyloxycarbonyl-2-(tert-butoxycarbonyl)-1-isopropyl-2-tosylhydrazine

: 286373-56-6
1-Benzyloxycarbonyl-2-(tert-butoxycarbonyl)-1-isopropylhydrazine

Guidance literature:: With magnesium; In methanol;
DOI:10.1039/b000139m

Reference yield:

: 286373-57-7
1-Benzyloxycarbonyl-2-(tert-butoxycarbonyl)-1-isopropyl-2-tosylhydrazine

: C₂₃H₂₉BrN₂O₄

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / Mg / methanol

2: 89 percent / tetrabutylammonium hydrogen sulfate; K₂CO₃ / acetonitrile / 24 h / 50 °C

With tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate; magnesium; In methanol; acetonitrile; 1: Substitution / 2: Alkylation;
DOI:10.1039/b000139m