2-allyl-4-bromophenyl ethyl allylphosphonate

Base Information

Chemical Name:2-allyl-4-bromophenyl ethyl allylphosphonate
CAS No.:1558056-36-2
Molecular Formula:C₁₄H₁₈BrO₃P
Molecular Weight:345.173
Hs Code.:

Synonyms:2-allyl-4-bromophenyl ethyl allylphosphonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-allyl-4-bromophenyl ethyl allylphosphonate

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Technology Process of 2-allyl-4-bromophenyl ethyl allylphosphonate

There total 2 articles about 2-allyl-4-bromophenyl ethyl allylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 41760-96-7
2-propenyl-phosphonochloridic acid, ethyl ester

: 13997-74-5
2-allyl-4-bromophenol

: 1558056-36-2
2-allyl-4-bromophenyl ethyl allylphosphonate

Guidance literature:: With triethylamine; In diethyl ether; at 0 - 20 ℃; for 4h; Inert atmosphere; Schlenk technique;
DOI:10.1016/j.tetlet.2014.01.008

Reference yield:

: 106-41-2
4-bromo-phenol

: 1558056-36-2
2-allyl-4-bromophenyl ethyl allylphosphonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / acetone / 8 h / Reflux; Inert atmosphere; Schlenk technique

1.2: 6 h / Reflux; Inert atmosphere; Schlenk technique

2.1: triethylamine / diethyl ether / 4 h / 0 - 20 °C / Inert atmosphere; Schlenk technique

With potassium carbonate; triethylamine; In diethyl ether; acetone;
DOI:10.1016/j.tetlet.2014.01.008