3,19-di(2-(4-(2,6-dichlorophenylamino)phenyl)acetyl)isoandrographolide

Base Information

Chemical Name:3,19-di(2-(4-(2,6-dichlorophenylamino)phenyl)acetyl)isoandrographolide
CAS No.:950895-55-3
Molecular Formula:C₄₈H₄₈Cl₄N₂O₇
Molecular Weight:906.73
Hs Code.:

Synonyms:3,19-di(2-(4-(2,6-dichlorophenylamino)phenyl)acetyl)isoandrographolide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,19-di(2-(4-(2,6-dichlorophenylamino)phenyl)acetyl)isoandrographolide

Chemical Property:

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Technology Process of 3,19-di(2-(4-(2,6-dichlorophenylamino)phenyl)acetyl)isoandrographolide

There total 2 articles about 3,19-di(2-(4-(2,6-dichlorophenylamino)phenyl)acetyl)isoandrographolide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 131663-98-4
C₁₄H₁₁Cl₂NO₂

: 4176-96-9
isoandrographolide

: 950895-55-3
3,19-di(2-(4-(2,6-dichlorophenylamino)phenyl)acetyl)isoandrographolide

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 0 - 20 ℃; for 10h;
DOI:10.2174/1573406411006040252

Reference yield:

: 142037-79-4,5508-58-7
andrographolide

: 950895-55-3
3,19-di(2-(4-(2,6-dichlorophenylamino)phenyl)acetyl)isoandrographolide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / water / 24 h / 20 °C

2: dmap; dicyclohexyl-carbodiimide / dichloromethane / 10 h / 0 - 20 °C

With hydrogenchloride; dmap; dicyclohexyl-carbodiimide; In dichloromethane; water;
DOI:10.2174/1573406411006040252