(+)-dimethyl 2-(4-methoxyphenyl)-3-(3-methyl-4-nitroisoxazol-5-yl)cyclopropane-1,1-dicarboxylate

Base Information

Chemical Name:(+)-dimethyl 2-(4-methoxyphenyl)-3-(3-methyl-4-nitroisoxazol-5-yl)cyclopropane-1,1-dicarboxylate
CAS No.:1371645-01-0
Molecular Formula:C₁₈H₁₈N₂O₈
Molecular Weight:390.35
Hs Code.:

Synonyms:(+)-dimethyl 2-(4-methoxyphenyl)-3-(3-methyl-4-nitroisoxazol-5-yl)cyclopropane-1,1-dicarboxylate

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Chemical Property of (+)-dimethyl 2-(4-methoxyphenyl)-3-(3-methyl-4-nitroisoxazol-5-yl)cyclopropane-1,1-dicarboxylate

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Technology Process of (+)-dimethyl 2-(4-methoxyphenyl)-3-(3-methyl-4-nitroisoxazol-5-yl)cyclopropane-1,1-dicarboxylate

There total 1 articles about (+)-dimethyl 2-(4-methoxyphenyl)-3-(3-methyl-4-nitroisoxazol-5-yl)cyclopropane-1,1-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 51978-98-4,53557-95-2
5-[(E)-2-(4-methoxyphenyl)-1-ethenyl]-3-methyl-4-nitroisoxazole

: 868-26-8
dimethyl 2-bromomalonate

: 1371645-01-0
(+)-dimethyl 2-(4-methoxyphenyl)-3-(3-methyl-4-nitroisoxazol-5-yl)cyclopropane-1,1-dicarboxylate

Guidance literature:: With potassium phosphate; N-(2-methoxybenzyl)quinidinium bromide; In water; toluene; at -37 ℃; for 42h; optical yield given as %ee; enantioselective reaction;
DOI:10.1039/c2cc30401e

Reference yield:

: 1371645-01-0
(+)-dimethyl 2-(4-methoxyphenyl)-3-(3-methyl-4-nitroisoxazol-5-yl)cyclopropane-1,1-dicarboxylate

: C₁₅H₁₆O₇

Guidance literature:: With potassium permanganate; water; In tetrahydrofuran; acetone; at 20 ℃; for 1h;
DOI:10.1039/c2cc30401e

Reference yield:

: 1371645-01-0
(+)-dimethyl 2-(4-methoxyphenyl)-3-(3-methyl-4-nitroisoxazol-5-yl)cyclopropane-1,1-dicarboxylate

: (+)-trimethyl 3-(4-methoxyphenyl)cyclopropane-1,1,2-tricarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium permanganate; water / tetrahydrofuran; acetone / 1 h / 20 °C

2: methanol; diethyl ether / 20 °C

With potassium permanganate; water; In tetrahydrofuran; methanol; diethyl ether; acetone;
DOI:10.1039/c2cc30401e