N-(2,2-diethoxyethyl)-N-(1,4-dimethyl-9H-carbazol-3-ylmethyl)-4-methylbenzenesulfonamide

Base Information

Chemical Name:N-(2,2-diethoxyethyl)-N-(1,4-dimethyl-9H-carbazol-3-ylmethyl)-4-methylbenzenesulfonamide
CAS No.:65266-48-0
Molecular Formula:C₂₈H₃₄N₂O₄S
Molecular Weight:494.655
Hs Code.:

Synonyms:N-(2,2-diethoxyethyl)-N-(1,4-dimethyl-9H-carbazol-3-ylmethyl)-4-methylbenzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(2,2-diethoxyethyl)-N-(1,4-dimethyl-9H-carbazol-3-ylmethyl)-4-methylbenzenesulfonamide

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Technology Process of N-(2,2-diethoxyethyl)-N-(1,4-dimethyl-9H-carbazol-3-ylmethyl)-4-methylbenzenesulfonamide

There total 29 articles about N-(2,2-diethoxyethyl)-N-(1,4-dimethyl-9H-carbazol-3-ylmethyl)-4-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 65266-47-9
N-(1,4-dimethylcarbazol-3-ylmethyl) aminoacetaldehyde diethyl acetal

: 98-59-9
p-toluenesulfonyl chloride

: 65266-48-0
N-(2,2-diethoxyethyl)-N-(1,4-dimethyl-9H-carbazol-3-ylmethyl)-4-methylbenzenesulfonamide

Guidance literature:: With triethylamine; In ethyl acetate; at 20 ℃; for 2h;
DOI:10.1002/jhet.319

Reference yield:

: 18028-55-2
1,4-dimethyl-9H-carbazole

: 65266-48-0
N-(2,2-diethoxyethyl)-N-(1,4-dimethyl-9H-carbazol-3-ylmethyl)-4-methylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1: 46 percent / POCl₃ / various solvent(s) / 5 h / Heating

2: 82.7 percent / 2 h / 100 °C

3: 74.6 percent / H₂ / Raney nickel / ethanol / 24 h / 20 °C / 6080 Torr

4: 92 percent / pyridine / 72 h / 20 °C

With hydrogen; trichlorophosphate; nickel; In pyridine; ethanol; 1: Formylation / 2: Condensation / 3: Hydrogenation / 4: Tosylation;
DOI:10.1007/BF02494860

Reference yield:

: 14501-66-7
1,4-dimethylcarbazole-3-carboxaldehyde

: 65266-48-0
N-(2,2-diethoxyethyl)-N-(1,4-dimethyl-9H-carbazol-3-ylmethyl)-4-methylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: 82.7 percent / 2 h / 100 °C

2: 74.6 percent / H₂ / Raney nickel / ethanol / 6080 Torr / Ambient temperature

3: 92 percent / pyridine / 72 h / Ambient temperature

With pyridine; hydrogen; nickel; In ethanol;
DOI:10.1007/BF00630657