diallyl α-fluoro-(α-phenylthio)-3-butenylphosphonate

Base Information

Chemical Name:diallyl α-fluoro-(α-phenylthio)-3-butenylphosphonate
CAS No.:870193-86-5
Molecular Formula:C₁₆H₂₀FO₃PS
Molecular Weight:342.371
Hs Code.:

Synonyms:diallyl α-fluoro-(α-phenylthio)-3-butenylphosphonate

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Chemical Property of diallyl α-fluoro-(α-phenylthio)-3-butenylphosphonate

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Technology Process of diallyl α-fluoro-(α-phenylthio)-3-butenylphosphonate

There total 5 articles about diallyl α-fluoro-(α-phenylthio)-3-butenylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 870193-91-2
diallyl 1-phenylthio-3-butenylphosphonate

: 870193-86-5
diallyl α-fluoro-(α-phenylthio)-3-butenylphosphonate

Guidance literature:: With tetraethylammonium fluoride; In 1,2-dimethoxyethane; at 20 ℃; Electrolysis;
DOI:10.1021/jo051206r

Reference yield:

: 38066-16-9
diethyl [(phenylthio)methyl]phosphonate

: 870193-86-5
diallyl α-fluoro-(α-phenylthio)-3-butenylphosphonate

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / n-BuLi

2: 65 percent / TMSBr; (COCl)2

3: 53 percent / Et₄NF*3HF / 1,2-dimethoxy-ethane / 20 °C / Electrolysis

With n-butyllithium; oxalyl dichloride; trimethylsilyl bromide; tetraethylammonium fluoride; In 1,2-dimethoxyethane;
DOI:10.1021/jo051206r

Reference yield:

: 10419-77-9
diethyl iodomethanephosphonate

: 870193-86-5
diallyl α-fluoro-(α-phenylthio)-3-butenylphosphonate

Guidance literature:: Multi-step reaction with 4 steps

1: KOH / ethanol / 5 h

2: 73 percent / n-BuLi

3: 65 percent / TMSBr; (COCl)2

4: 53 percent / Et₄NF*3HF / 1,2-dimethoxy-ethane / 20 °C / Electrolysis

With potassium hydroxide; n-butyllithium; oxalyl dichloride; trimethylsilyl bromide; tetraethylammonium fluoride; In 1,2-dimethoxyethane; ethanol;
DOI:10.1021/jo051206r