Technology Process of 2,3-O-isopropylidene-2-hydroxymethyl-L-erythrose
There total 1 articles about 2,3-O-isopropylidene-2-hydroxymethyl-L-erythrose which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
methanol;
for 4h;
Reflux;
DOI:10.1021/ja201769f
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 1H-imidazole / dichloromethane / 2 h / 20 °C
2.1: n-butyllithium / tetrahydrofuran / 0.33 h / 0 °C
2.2: 3 h / 20 °C
3.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / tetrahydrofuran; water; tert-butyl alcohol / 48 h / 20 °C
4.1: 1H-imidazole / dichloromethane / 2 h / 20 °C
With
1H-imidazole; osmium(VIII) oxide; n-butyllithium; 4-methylmorpholine N-oxide;
In
tetrahydrofuran; dichloromethane; water; tert-butyl alcohol;
DOI:10.1021/ja201769f
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 1H-imidazole / dichloromethane / 2 h / 20 °C
2.1: n-butyllithium / tetrahydrofuran / 0.33 h / 0 °C
2.2: 3 h / 20 °C
3.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / tetrahydrofuran; water; tert-butyl alcohol / 48 h / 20 °C
4.1: 1H-imidazole / dichloromethane / 2 h / 20 °C
5.1: dipyridinium dichromate; acetic anhydride / dichloromethane / 3 h / Reflux
With
1H-imidazole; osmium(VIII) oxide; dipyridinium dichromate; n-butyllithium; acetic anhydride; 4-methylmorpholine N-oxide;
In
tetrahydrofuran; dichloromethane; water; tert-butyl alcohol;
DOI:10.1021/ja201769f
