[(1,3-bis(diphenylphosphino)propane)]platinum(II)(3-methoxy-2,3-propanediolate)

Base Information

Chemical Name:[(1,3-bis(diphenylphosphino)propane)]platinum(II)(3-methoxy-2,3-propanediolate)
CAS No.:156053-63-3
Molecular Formula:C₃₁H₃₄O₃P₂Pt
Molecular Weight:711.637
Hs Code.:

Synonyms:[(1,3-bis(diphenylphosphino)propane)]platinum(II)(3-methoxy-2,3-propanediolate)

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Chemical Property of [(1,3-bis(diphenylphosphino)propane)]platinum(II)(3-methoxy-2,3-propanediolate)

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Technology Process of [(1,3-bis(diphenylphosphino)propane)]platinum(II)(3-methoxy-2,3-propanediolate)

There total 3 articles about [(1,3-bis(diphenylphosphino)propane)]platinum(II)(3-methoxy-2,3-propanediolate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 156053-80-4
(1,3-bis(diphenylphosphino)propane)Pt(CO₃)

: 623-39-2,36887-04-4
glycerol 1-monomethyl ether

: 156053-63-3
[(1,3-bis(diphenylphosphino)propane)]platinum(II)(3-methoxy-2,3-propanediolate)

Guidance literature:: In dichloromethane; byproducts: CO2, H2O; under Ar; Pt-complex and excess diol dissolved in CH2Cl2, soln. stirred with periodic purging with Ar; react. readily reversed by treatment with dry ice; evapn. (vac.), dried, powder washed with min. amt. H2O (removal of excess diol), dried (vac.), dissolved in min. amt. CH2Cl2, layered with Et2O, diffusion (crystn.), washed (Et2O), dried (vac.), elem. anal.;
DOI:10.1021/ja00092a025

Reference yield:

: 59329-00-9
[1,3-bis(diphenylphosphino)propane]dichloroplatinum(II)

: 156053-63-3
[(1,3-bis(diphenylphosphino)propane)]platinum(II)(3-methoxy-2,3-propanediolate)

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran

2: CO₂ / tetrahydrofuran; water

3: dichloromethane

With CO₂; In tetrahydrofuran; dichloromethane; water;
DOI:10.1021/ja00092a025

Reference yield:

: 156053-79-1
[(C₆H₅)2PCH₂CH₂CH₂P(C₆H₅)2]Pt[OCH(CH₃)2]2

: 156053-63-3
[(1,3-bis(diphenylphosphino)propane)]platinum(II)(3-methoxy-2,3-propanediolate)

Guidance literature:: Multi-step reaction with 2 steps

1: CO₂ / tetrahydrofuran; water

2: dichloromethane

With CO₂; In tetrahydrofuran; dichloromethane; water;
DOI:10.1021/ja00092a025