6-(3-nitro-1,2,4-triazol-1-yl)-9-<3',5'-di-O-benzoyl-2'-O-(tetrahydropyran-2-yl)-β-D-ribofuranosyl>-9H-purine

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Chemical Name:6-(3-nitro-1,2,4-triazol-1-yl)-9-<3',5'-di-O-benzoyl-2'-O-(tetrahydropyran-2-yl)-β-D-ribofuranosyl>-9H-purine
CAS No.:161834-99-7
Molecular Formula:C₃₁H₂₈N₈O₉
Molecular Weight:656.612
Hs Code.:

Synonyms:6-(3-nitro-1,2,4-triazol-1-yl)-9-<3',5'-di-O-benzoyl-2'-O-(tetrahydropyran-2-yl)-β-D-ribofuranosyl>-9H-purine

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Chemical Property of 6-(3-nitro-1,2,4-triazol-1-yl)-9-<3',5'-di-O-benzoyl-2'-O-(tetrahydropyran-2-yl)-β-D-ribofuranosyl>-9H-purine

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Technology Process of 6-(3-nitro-1,2,4-triazol-1-yl)-9-<3',5'-di-O-benzoyl-2'-O-(tetrahydropyran-2-yl)-β-D-ribofuranosyl>-9H-purine

There total 1 articles about 6-(3-nitro-1,2,4-triazol-1-yl)-9-<3',5'-di-O-benzoyl-2'-O-(tetrahydropyran-2-yl)-β-D-ribofuranosyl>-9H-purine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 24807-55-4
3-nitro-1,2,4-triazole

: 3',5'-di-O-benzoyl-2'-O-(tetrahydropyran-2-yl)inosine

: 161834-99-7
6-(3-nitro-1,2,4-triazol-1-yl)-9-<3',5'-di-O-benzoyl-2'-O-(tetrahydropyran-2-yl)-β-D-ribofuranosyl>-9H-purine

Guidance literature:: With diphenyl hydrogen phosphate; p-toluenesulfonyl chloride; In pyridine; at 50 ℃; for 24.75h;
DOI:10.1080/07328319608002421

Reference yield:

: 161834-99-7
6-(3-nitro-1,2,4-triazol-1-yl)-9-<3',5'-di-O-benzoyl-2'-O-(tetrahydropyran-2-yl)-β-D-ribofuranosyl>-9H-purine

: 3',5'-di-O-benzoyl-N⁶-succinyl-2'-O-(tetrahydropyran-2-yl)adenosine

Guidance literature:: Multi-step reaction with 2 steps

1: DBU / CH₂Cl₂ / 24 h / Ambient temperature

2: Ac₂O, Et₃N / CH₂Cl₂ / 1 h / Ambient temperature

With acetic anhydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In dichloromethane;
DOI:10.1016/0040-4039(94)02173-9

Reference yield:

: 161834-99-7
6-(3-nitro-1,2,4-triazol-1-yl)-9-<3',5'-di-O-benzoyl-2'-O-(tetrahydropyran-2-yl)-β-D-ribofuranosyl>-9H-purine

: 3',5'-di-O-benzoyl-N⁶-phthaloyl-2'-O-(tetrahydropyran-2-yl)adenosine

Guidance literature:: Multi-step reaction with 2 steps

1: DBU / CH₂Cl₂ / 24 h / Ambient temperature

2: Ac₂O, Et₃N / CH₂Cl₂ / 1 h / Ambient temperature

With acetic anhydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In dichloromethane;
DOI:10.1016/0040-4039(94)02173-9