Welcome to LookChem.com Sign In|Join Free
  • or

Encyclopedia

Technology Process of Re(C5(CH3)5)(N2C6H4OCH3)(CO)Br

Re(C5(CH3)5)(N2C6H4OCH3)(CO)Br

Base Information
  • Chemical Name:Re(C5(CH3)5)(N2C6H4OCH3)(CO)Br
  • CAS No.:92786-95-3
  • Molecular Formula:C18H22BrN2O2Re
  • Molecular Weight:564.496
  • Hs Code.:
Re(C<sub>5</sub>(CH<sub>3</sub>)5)(N<sub>2</sub>C<sub>6</sub>H<sub>4</sub>OCH<sub>3</sub>)(CO)Br

Synonyms:Re(C5(CH3)5)(N2C6H4OCH3)(CO)Br

Suppliers and Price of Re(C5(CH3)5)(N2C6H4OCH3)(CO)Br
Supply Marketing:
Business phase:
The product has achieved commercial mass production*data from LookChem market partment
Manufacturers and distributors:
  • Manufacture/Brand
  • Chemicals and raw materials
  • Packaging
  • price
Total 2 raw suppliers
Chemical Property of Re(C5(CH3)5)(N2C6H4OCH3)(CO)Br
Chemical Property:
Purity/Quality:

98% *data from raw suppliers

Safty Information:
  • Pictogram(s):  
  • Hazard Codes: 
MSDS Files:
Useful:
Technology Process of Re(C5(CH3)5)(N2C6H4OCH3)(CO)Br

There total 2 articles about Re(C5(CH3)5)(N2C6H4OCH3)(CO)Br which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

{Cp*Re(CO)2(p-N<sub>2</sub>C<sub>6</sub>H<sub>4</sub>OMe)}{BF<sub>4</sub>}
92786-90-8

{Cp*Re(CO)2(p-N2C6H4OMe)}{BF4}

pentamethylcyclopentadienyltrioxorhenium

pentamethylcyclopentadienyltrioxorhenium

Re(C<sub>5</sub>(CH<sub>3</sub>)5)(N<sub>2</sub>C<sub>6</sub>H<sub>4</sub>OCH<sub>3</sub>)(CO)Br
92786-95-3

Re(C5(CH3)5)(N2C6H4OCH3)(CO)Br

Guidance literature:
With potassium bromide; In tetrahydrofuran; water; Schlenk app., N2; Re compd. is stirred with excess KBr in THF-H2O for 36 h; THF is removed in vac., H2O is decanted, solid is dissolved in THF and chromd. (Florisil), monobromo compd. (elem. anal.) from the red fractionwith THF-hexane, Cp(*)ReO3 from yellow fraction with THF-hexane and pptn. with hexane at low temp.;

Reference yield:

{Cp*Re(CO)2(p-N<sub>2</sub>C<sub>6</sub>H<sub>4</sub>OMe)}{BF<sub>4</sub>}
92786-90-8

{Cp*Re(CO)2(p-N2C6H4OMe)}{BF4}

cis-(η(5)-pentamethylcyclopentadienyl)(dibromo)(dicarbonyl)rhenium

cis-(η(5)-pentamethylcyclopentadienyl)(dibromo)(dicarbonyl)rhenium

Re(C<sub>5</sub>(CH<sub>3</sub>)5)(N<sub>2</sub>C<sub>6</sub>H<sub>4</sub>OCH<sub>3</sub>)(CO)Br
92786-95-3

Re(C5(CH3)5)(N2C6H4OCH3)(CO)Br

Guidance literature:
With potassium bromide; In solid; Schlenk app., N2; Re compd. is ground with solid KBr, mixt. is heated at 95°C for 4 h; extd. with CH2Cl2, then chromd. (silica gel): monobromo compd. from orange-red band with CH2Cl2-hexane, dibromo compd. from further fraction with CH2Cl2 (IR);
upstream raw materials:

{Cp*Re(CO)2(p-N2C6H4OMe)}{BF4}

Post a RFQ

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

1 Customer Service

What can I do for you?
Get Best Price

Get Best Price for 92786-95-3

Total 8 Pictures about this product