3-amino-5-fluoro-2-methyl-benzoic acid

Base Information

Chemical Name:3-amino-5-fluoro-2-methyl-benzoic acid
CAS No.:246877-31-6
Molecular Formula:C₈H₈FNO₂
Molecular Weight:169.155
Hs Code.:

Synonyms:3-amino-5-fluoro-2-methylbenzoic acid

Suppliers and Price of 3-amino-5-fluoro-2-methyl-benzoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
3-Amino-5-fluoro-2-methylbenzoicacid 95+%
10g
$ 465.00

Crysdot
3-Amino-5-fluoro-2-methylbenzoicacid 95+%
5g
$ 372.00

Crysdot
3-Amino-5-fluoro-2-methylbenzoicacid 95+%
25g
$ 842.00

Chemcia Scientific
3-Amino-5-fluoro-2-methyl-benzoicacid 95%
5 G
$ 995.00

Alichem
3-Amino-5-fluoro-2-methylbenzoicacid
25g
$ 1266.30

Alichem
3-Amino-5-fluoro-2-methylbenzoicacid
10g
$ 683.40

Alichem
3-Amino-5-fluoro-2-methylbenzoicacid
5g
$ 573.52

Total 2 raw suppliers

Chemical Property of 3-amino-5-fluoro-2-methyl-benzoic acid

Chemical Property:

Purity/Quality:

≥99% ^*data from raw suppliers

3-Amino-5-fluoro-2-methylbenzoicacid 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-amino-5-fluoro-2-methyl-benzoic acid

There total 3 articles about 3-amino-5-fluoro-2-methyl-benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 246877-30-5
5-fluoro-2-methyl-3-nitrobenzoic acid benzyl ester

: 246877-31-6
3-amino-5-fluoro-2-methylbenzoic acid

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; at 20 ℃; for 41.5h;

Reference yield:

: 850462-64-5
5-fluoro-2-methyl-3-nitrobenzoic acid

: 246877-31-6
3-amino-5-fluoro-2-methylbenzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 41 percent / K₂CO₃ / 1 h / 50 °C

2: 257 mg / H₂ / 10 percent Pd-C / 20 h / 20 °C / 760 Torr

With hydrogen; potassium carbonate; palladium on activated charcoal; 1: Esterification / 2: Catalytic hydrogenation;
DOI:10.1016/S0968-0896(99)00127-3

Reference yield:

: 33184-16-6
5-fluoro-2-methylbenzoic acid

: 246877-31-6
3-amino-5-fluoro-2-methylbenzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: HNO₃; H₂SO₄ / 0.5 h / 0 °C

2: 41 percent / K₂CO₃ / 1 h / 50 °C

3: 257 mg / H₂ / 10 percent Pd-C / 20 h / 20 °C / 760 Torr

With sulfuric acid; hydrogen; nitric acid; potassium carbonate; palladium on activated charcoal; 1: Nitration / 2: Esterification / 3: Catalytic hydrogenation;
DOI:10.1016/S0968-0896(99)00127-3