1D-(1,2,4/3,5)-2-acetamido-1,4,5-tri-O-acetyl-3-O-<(R)-1'-carboxyethyl>-1,3,4,5-cyclohexanetetrol

Base Information

Chemical Name:1D-(1,2,4/3,5)-2-acetamido-1,4,5-tri-O-acetyl-3-O-<(R)-1'-carboxyethyl>-1,3,4,5-cyclohexanetetrol
CAS No.:121788-66-7
Molecular Formula:C₁₇H₂₅NO₁₀
Molecular Weight:403.386
Hs Code.:

Synonyms:1D-(1,2,4/3,5)-2-acetamido-1,4,5-tri-O-acetyl-3-O-<(R)-1'-carboxyethyl>-1,3,4,5-cyclohexanetetrol

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Chemical Property of 1D-(1,2,4/3,5)-2-acetamido-1,4,5-tri-O-acetyl-3-O-<(R)-1'-carboxyethyl>-1,3,4,5-cyclohexanetetrol

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Technology Process of 1D-(1,2,4/3,5)-2-acetamido-1,4,5-tri-O-acetyl-3-O-<(R)-1'-carboxyethyl>-1,3,4,5-cyclohexanetetrol

There total 10 articles about 1D-(1,2,4/3,5)-2-acetamido-1,4,5-tri-O-acetyl-3-O-<(R)-1'-carboxyethyl>-1,3,4,5-cyclohexanetetrol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 121788-65-6
1D-(1,2,4/3,5)-2-acetamido-1,4,5-tri-O-acetyl-3-O-<(R)-1'-benzylcarboxyethyl>-1,3,4,5-cyclohexanetetrol

: 121788-66-7
1D-(1,2,4/3,5)-2-acetamido-1,4,5-tri-O-acetyl-3-O-<(R)-1'-carboxyethyl>-1,3,4,5-cyclohexanetetrol

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; for 2h; under 1500.1 Torr;
DOI:10.1016/S0040-4020(01)97594-5

Reference yield:

: 121843-61-6
methyl 2-acetamido-4-O-acetyl-3-O-<(R)-1'-benzylcarboxyethyl>-2-deoxy-α,β-D-xylo-hex-5-enopyranoside

: 121788-66-7
1D-(1,2,4/3,5)-2-acetamido-1,4,5-tri-O-acetyl-3-O-<(R)-1'-carboxyethyl>-1,3,4,5-cyclohexanetetrol

Guidance literature:: Multi-step reaction with 3 steps

1: HgSO₄, 5 mM H₂SO₄ / dioxane; H₂O / 2 h / 80 °C

2: 1.) lithium tert-butoxyaluminium hydride / 1.) THF, 0 deg C

3: H₂ / 10percent Pd/C / ethanol

With sulfuric acid; hydrogen; mercury(II) sulfate; lithium tri-t-butoxyaluminum hydride; palladium on activated charcoal; In 1,4-dioxane; ethanol; water;
DOI:10.1021/jo00277a002

Reference yield:

: 121843-60-5
methyl 2-acetamido-4-O-acetyl-3-O-<(R)-1'-benzylcarboxyethyl>-2,6-dideoxy-6-iodo-α,β-D-glucopyranoside

: 121788-66-7
1D-(1,2,4/3,5)-2-acetamido-1,4,5-tri-O-acetyl-3-O-<(R)-1'-carboxyethyl>-1,3,4,5-cyclohexanetetrol

Guidance literature:: Multi-step reaction with 4 steps

1: AgF, pyridine

2: HgSO₄, 5 mM H₂SO₄ / dioxane; H₂O / 2 h / 80 °C

3: 1.) lithium tert-butoxyaluminium hydride / 1.) THF, 0 deg C

4: H₂ / 10percent Pd/C / ethanol

With pyridine; sulfuric acid; hydrogen; silver fluoride; mercury(II) sulfate; lithium tri-t-butoxyaluminum hydride; palladium on activated charcoal; In 1,4-dioxane; ethanol; water;
DOI:10.1021/jo00277a002